methyl 4'-((3-butyl-1-(2,6-dichlorophenyl)-5-oxo-1H-[1,2,4]triazol-4(5H)-yl)methyl)biphenyl-2-carboxylate

Base Information

• Chemical Name: methyl 4'-((3-butyl-1-(2,6-dichlorophenyl)-5-oxo-1H-[1,2,4]triazol-4(5H)-yl)methyl)biphenyl-2-carboxylate
• CAS No.: 1206199-86-1
• Molecular Formula: C₂₇H₂₅Cl₂N₃O₃
• Molecular Weight: 510.42

Synonyms:methyl 4'-((3-butyl-1-(2,6-dichlorophenyl)-5-oxo-1H-[1,2,4]triazol-4(5H)-yl)methyl)biphenyl-2-carboxylate

Chemical Property of methyl 4'-((3-butyl-1-(2,6-dichlorophenyl)-5-oxo-1H-[1,2,4]triazol-4(5H)-yl)methyl)biphenyl-2-carboxylate

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Technology Process of methyl 4'-((3-butyl-1-(2,6-dichlorophenyl)-5-oxo-1H-[1,2,4]triazol-4(5H)-yl)methyl)biphenyl-2-carboxylate

There total 1 articles about methyl 4'-((3-butyl-1-(2,6-dichlorophenyl)-5-oxo-1H-[1,2,4]triazol-4(5H)-yl)methyl)biphenyl-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Methyl 4'-(bromomethyl)biphenyl-2-carboxylate (114772-38-2) + 5-Butyl-2-(2,6-dichloro-phenyl)-2,4-dihydro-[1,2,4]triazol-3-one (862261-61-8) → methyl 4'-((3-butyl-1-(2,6-dichlorophenyl)-5-oxo-1H-[1,2,4]triazol-4(5H)-yl)methyl)biphenyl-2-carboxylate (1206199-86-1)

Guidance literature:

5-Butyl-2-(2,6-dichloro-phenyl)-2,4-dihydro-[1,2,4]triazol-3-one; With sodium hydride; In N,N-dimethyl-formamide; at 30 ℃; Inert atmosphere;

Methyl 4'-(bromomethyl)biphenyl-2-carboxylate; In N,N-dimethyl-formamide; at 30 ℃; for 3.5h; Inert atmosphere;

DOI:10.2174/157018010789869370

Reference yield: 56.6%

methyl 4'-((3-butyl-1-(2,6-dichlorophenyl)-5-oxo-1H-[1,2,4]triazol-4(5H)-yl)methyl)biphenyl-2-carboxylate (1206199-86-1) → 4'-((3-butyl-1-(2,6-dichlorophenyl)-5-oxo-1H-[1,2,4]triazol-4(5H)-yl)methyl)biphenyl-2-carboxylic acid (1206199-85-0)

Guidance literature:

With water; sodium hydroxide; In methanol; Reflux;

DOI:10.2174/157018010789869370

upstream raw materials:

Methyl 4'-(bromomethyl)biphenyl-2-carboxylate

5-Butyl-2-(2,6-dichloro-phenyl)-2,4-dihydro-[1,2,4]triazol-3-one

Downstream raw materials:

4'-((3-butyl-1-(2,6-dichlorophenyl)-5-oxo-1H-[1,2,4]triazol-4(5H)-yl)methyl)biphenyl-2-carboxylic acid

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