N,N'-bis(2-t-butylthiobenzyl)ethylenediamine-N,N'-diacetic acid, di-t-butyl ester

Base Information

• Chemical Name: N,N'-bis(2-t-butylthiobenzyl)ethylenediamine-N,N'-diacetic acid, di-t-butyl ester
• CAS No.: 226383-43-3
• Molecular Formula: C₃₆H₅₆N₂O₄S₂
• Molecular Weight: 644.984

Synonyms:N,N'-bis(2-t-butylthiobenzyl)ethylenediamine-N,N'-diacetic acid, di-t-butyl ester

Chemical Property of N,N'-bis(2-t-butylthiobenzyl)ethylenediamine-N,N'-diacetic acid, di-t-butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of N,N'-bis(2-t-butylthiobenzyl)ethylenediamine-N,N'-diacetic acid, di-t-butyl ester

There total 2 articles about N,N'-bis(2-t-butylthiobenzyl)ethylenediamine-N,N'-diacetic acid, di-t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

bromoacetic acid tert-butyl ester (5292-43-3) + N,N'-bis(2-(tert-butylthio)benzyl)ethane-1,2-diamine (226383-42-2) → N,N'-bis(2-t-butylthiobenzyl)ethylenediamine-N,N'-diacetic acid, di-t-butyl ester (226383-43-3)

Guidance literature:

With potassium carbonate; potassium iodide; In acetonitrile; for 24h; Ambient temperature;

DOI:10.1016/S0040-4020(99)00243-4

Reference yield:

N,N'-bis([2-(1,1-dimethylethylthio)phenyl]methylene)-ethane-1,2-diamine (123746-54-3) → N,N'-bis(2-t-butylthiobenzyl)ethylenediamine-N,N'-diacetic acid, di-t-butyl ester (226383-43-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / NaBH₃CN, conc. HCl / ethanol / 2 h / Ambient temperature

2: 79 percent / K₂CO₃, KI / acetonitrile / 24 h / Ambient temperature

With hydrogenchloride; sodium cyanoborohydride; potassium carbonate; potassium iodide; In ethanol; acetonitrile;

DOI:10.1016/S0040-4020(99)00243-4

Reference yield: 90.0%

N,N'-bis(2-t-butylthiobenzyl)ethylenediamine-N,N'-diacetic acid, di-t-butyl ester (226383-43-3) → N,N'-bis(2-t-butylthiobenzyl)ethylenediamine-N,N'-diacetic acid (226383-45-5)

Guidance literature:

With trifluoroacetic acid; for 48h; Ambient temperature;

DOI:10.1016/S0040-4020(99)00243-4

upstream raw materials:

bromoacetic acid tert-butyl ester

N,N'-bis(2-(tert-butylthio)benzyl)ethane-1,2-diamine

N,N'-bis([2-(1,1-dimethylethylthio)phenyl]methylene)-ethane-1,2-diamine

Downstream raw materials:

N,N'-bis(2-t-butylthiobenzyl)ethylenediamine-N,N'-diacetic acid

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