4-(benzoylamino)cyclooctanone ethylene acetal

Base Information

Chemical Name:4-(benzoylamino)cyclooctanone ethylene acetal
CAS No.:159853-44-8
Molecular Formula:C₁₇H₂₃NO₃
Molecular Weight:289.375
Hs Code.:

Synonyms:4-(benzoylamino)cyclooctanone ethylene acetal

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Chemical Property of 4-(benzoylamino)cyclooctanone ethylene acetal

Chemical Property:

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Technology Process of 4-(benzoylamino)cyclooctanone ethylene acetal

There total 1 articles about 4-(benzoylamino)cyclooctanone ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 16801-73-3
4-(benzoylamino)cyclooctanone

: 107-21-1
ethylene glycol

: 159853-44-8
4-(benzoylamino)cyclooctanone ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 3h; Heating;
DOI:10.1016/S0040-4020(01)85713-6

Reference yield: 99.0%

: 159853-44-8
4-(benzoylamino)cyclooctanone ethylene acetal

: 159853-45-9
4-(benzylamino)cyclooctanone ethylene acetal

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 24h; Heating;
DOI:10.1016/S0040-4020(01)85713-6

Reference yield:

: 159853-44-8
4-(benzoylamino)cyclooctanone ethylene acetal

: 139535-28-7
4-(benzylamino)cyclooctanone

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / LiAlH₄ / tetrahydrofuran / 24 h / Heating

2: 95 percent / ethanoic acid / H₂O / 2 h / 90 °C

With lithium aluminium tetrahydride; acetic acid; In tetrahydrofuran; water;
DOI:10.1016/S0040-4020(01)85713-6