2-(4-Chloro-phenyl)-4,7-dimethyl-1a,4-dihydro-1-oxa-3,4,5,7-tetraaza-cyclopropa[d]naphthalene-6,8-dione

Base Information

• Chemical Name: 2-(4-Chloro-phenyl)-4,7-dimethyl-1a,4-dihydro-1-oxa-3,4,5,7-tetraaza-cyclopropa[d]naphthalene-6,8-dione
• CAS No.: 81976-06-9
• Molecular Formula: C₁₄H₁₁ClN₄O₃
• Molecular Weight: 318.719

Synonyms:2-(4-Chloro-phenyl)-4,7-dimethyl-1a,4-dihydro-1-oxa-3,4,5,7-tetraaza-cyclopropa[d]naphthalene-6,8-dione

Chemical Property of 2-(4-Chloro-phenyl)-4,7-dimethyl-1a,4-dihydro-1-oxa-3,4,5,7-tetraaza-cyclopropa[d]naphthalene-6,8-dione

Chemical Property:

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Technology Process of 2-(4-Chloro-phenyl)-4,7-dimethyl-1a,4-dihydro-1-oxa-3,4,5,7-tetraaza-cyclopropa[d]naphthalene-6,8-dione

There total 3 articles about 2-(4-Chloro-phenyl)-4,7-dimethyl-1a,4-dihydro-1-oxa-3,4,5,7-tetraaza-cyclopropa[d]naphthalene-6,8-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3-(4-chlorophenyl)-1,6-dimethylpyrimido[4,5-c]pyridazine-5,7(1H,6H)-dione (68871-18-1) → 2-(4-Chloro-phenyl)-4,7-dimethyl-1a,4-dihydro-1-oxa-3,4,5,7-tetraaza-cyclopropa[d]naphthalene-6,8-dione (81976-06-9)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 24h; Ambient temperature;

DOI:10.1248/cpb.30.172

Reference yield:

3-(4-Chloro-phenyl)-1-methyl-1H-pyrimido[4,5-c]pyridazine-5,7-dione (81976-00-3) → 2-(4-Chloro-phenyl)-4,7-dimethyl-1a,4-dihydro-1-oxa-3,4,5,7-tetraaza-cyclopropa[d]naphthalene-6,8-dione (81976-06-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / dimethylformamide / 3 h / 90 °C

2: 85 percent / m-chloroperbenzoic acid / CHCl₃ / 24 h / Ambient temperature

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In chloroform; N,N-dimethyl-formamide;

DOI:10.1248/cpb.30.172

Reference yield:

6-(1-methylhydrazino)uracil (68558-26-9) → 2-(4-Chloro-phenyl)-4,7-dimethyl-1a,4-dihydro-1-oxa-3,4,5,7-tetraaza-cyclopropa[d]naphthalene-6,8-dione (81976-06-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 52 percent / 2-methoxy-ethanol / 2 h / Heating

2: potassium carbonate / dimethylformamide / 3 h / 90 °C

3: 85 percent / m-chloroperbenzoic acid / CHCl₃ / 24 h / Ambient temperature

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In chloroform; 2-methoxy-ethanol; N,N-dimethyl-formamide;

DOI:10.1248/cpb.30.172

upstream raw materials:

3-(4-chlorophenyl)-1,6-dimethylpyrimido[4,5-c]pyridazine-5,7(1H,6H)-dione

3-(4-Chloro-phenyl)-1-methyl-1H-pyrimido[4,5-c]pyridazine-5,7-dione

6-(1-methylhydrazino)uracil

Downstream raw materials:

6-(4-Chloro-phenyl)-4-hydroxy-2-methyl-2H-pyridazin-3-one

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