thexyldimethylsilyl 4-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:thexyldimethylsilyl 4-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside
CAS No.:1426433-27-3
Molecular Formula:C₃₀H₄₃N₃O₆Si
Molecular Weight:569.773
Hs Code.:

Synonyms:thexyldimethylsilyl 4-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of thexyldimethylsilyl 4-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

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Technology Process of thexyldimethylsilyl 4-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

There total 8 articles about thexyldimethylsilyl 4-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 108-24-7
acetic anhydride

: 174077-02-2
dimethylthexylsilyl 3,6-di-O-benzyl-2-deoxy-2-azido-β-D-glucopyranoside

: 1426433-27-3
thexyldimethylsilyl 4-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With pyridine; dmap; at 0 - 20 ℃;
DOI:10.3998/ark.5550190.0014.214

Reference yield:

: thexyldimethylsilyl 2-azido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

: 1426433-27-3
thexyldimethylsilyl 4-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylsilane / dichloromethane / 0.5 h

1.2: 0 - 20 °C

2.1: dmap; pyridine / 0 - 20 °C

With pyridine; triethylsilane; dmap; In dichloromethane;
DOI:10.3998/ark.5550190.0014.214

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 1426433-27-3
thexyldimethylsilyl 4-O-acetyl-2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: camphor-10-sulfonic acid / acetonitrile / 72 h / 20 °C

2.1: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 1 h / 20 °C

3.1: triethylsilane / dichloromethane / 0.5 h

3.2: 0 - 20 °C

4.1: dmap; pyridine / 0 - 20 °C

With pyridine; triethylsilane; dmap; camphor-10-sulfonic acid; tetra-(n-butyl)ammonium iodide; sodium hydride; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.3998/ark.5550190.0014.214