diethyl N-(N-carbobenzyloxy-L-alanyl-β-2-thienyl-DL-alanyl)-1-aminoethylphosphonate

Base Information

Chemical Name:diethyl N-(N-carbobenzyloxy-L-alanyl-β-2-thienyl-DL-alanyl)-1-aminoethylphosphonate
CAS No.:81071-14-9
Molecular Formula:C₂₄H₃₄N₃O₇PS
Molecular Weight:539.59
Hs Code.:

Synonyms:diethyl N-(N-carbobenzyloxy-L-alanyl-β-2-thienyl-DL-alanyl)-1-aminoethylphosphonate

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Chemical Property of diethyl N-(N-carbobenzyloxy-L-alanyl-β-2-thienyl-DL-alanyl)-1-aminoethylphosphonate

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Technology Process of diethyl N-(N-carbobenzyloxy-L-alanyl-β-2-thienyl-DL-alanyl)-1-aminoethylphosphonate

There total 4 articles about diethyl N-(N-carbobenzyloxy-L-alanyl-β-2-thienyl-DL-alanyl)-1-aminoethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.9%

: 54788-35-1
diethyl 1-aminoethylphosphonate

: 81071-10-5
N-carbobenzyloxy-L-alanyl-β-2-thienyl-DL-alanine

: 81071-14-9
diethyl N-(N-carbobenzyloxy-L-alanyl-β-2-thienyl-DL-alanyl)-1-aminoethylphosphonate

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; for 17h;

Reference yield:

: 81071-08-1
β-2-thienyl-DL-alanine ethyl ester

: 81071-14-9
diethyl N-(N-carbobenzyloxy-L-alanyl-β-2-thienyl-DL-alanyl)-1-aminoethylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 95.7 percent / N-hydroxy-5-norbornene-2,3-dicarboxyimide, dicyclohexylcarbodiimide (DCC), Et₃N / CH₂Cl₂ / 18 h / 0 - 20 °C

2: 75.1 percent / NaOH / ethanol / 0.75 h / Ambient temperature

3: 69.9 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂; dimethylformamide / 17 h / 0 - 20 °C

With sodium hydroxide; N-hydroxy-5-norbornene-2,3-dicarboxyimide; triethylamine; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 81071-09-2
N-carbobenzyloxy-L-alanyl-β-2-thienyl-DL-alanine ethyl ester

: 81071-14-9
diethyl N-(N-carbobenzyloxy-L-alanyl-β-2-thienyl-DL-alanyl)-1-aminoethylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 75.1 percent / NaOH / ethanol / 0.75 h / Ambient temperature

2: 69.9 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂; dimethylformamide / 17 h / 0 - 20 °C

With sodium hydroxide; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; N,N-dimethyl-formamide;