N-(4-chlorophenyl)-3-(N-(4-chlorophenyl)-N-methylsulfamoyl)-4-hydroxybenzamide

Base Information

Chemical Name:N-(4-chlorophenyl)-3-(N-(4-chlorophenyl)-N-methylsulfamoyl)-4-hydroxybenzamide
CAS No.:1586822-74-3
Molecular Formula:C₂₀H₁₆Cl₂N₂O₄S
Molecular Weight:451.33
Hs Code.:

Synonyms:N-(4-chlorophenyl)-3-(N-(4-chlorophenyl)-N-methylsulfamoyl)-4-hydroxybenzamide

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Chemical Property of N-(4-chlorophenyl)-3-(N-(4-chlorophenyl)-N-methylsulfamoyl)-4-hydroxybenzamide

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Technology Process of N-(4-chlorophenyl)-3-(N-(4-chlorophenyl)-N-methylsulfamoyl)-4-hydroxybenzamide

There total 4 articles about N-(4-chlorophenyl)-3-(N-(4-chlorophenyl)-N-methylsulfamoyl)-4-hydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 361473-14-5
3-(N-(4-chlorophenyl)-N-methylsulfamoyl)benzoic acid

: 106-47-8
4-chloro-aniline

: 1586822-74-3
N-(4-chlorophenyl)-3-(N-(4-chlorophenyl)-N-methylsulfamoyl)-4-hydroxybenzamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;
DOI:10.1016/j.ejmech.2014.02.003

Reference yield: 83.0%

: 1586822-74-3
N-(4-chlorophenyl)-3-(N-(4-chlorophenyl)-N-methylsulfamoyl)-4-hydroxybenzamide

Guidance literature:: With boron tribromide; In dichloromethane; at 20 ℃; Inert atmosphere; Cooling with acetone-dry ice;

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 1586822-74-3
N-(4-chlorophenyl)-3-(N-(4-chlorophenyl)-N-methylsulfamoyl)-4-hydroxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 4 h / 65 °C

2: pyridine / ethyl acetate / 0 - 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With pyridine; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; ethyl acetate;
DOI:10.1016/j.ejmech.2014.02.003