2-<4-methyl-2-(methoxy)phenyl>-1-tetrahydro-2H-1,4-oxazin-4-yl-1-ethanthione

Base Information

• Chemical Name: 2-<4-methyl-2-(methoxy)phenyl>-1-tetrahydro-2H-1,4-oxazin-4-yl-1-ethanthione
• CAS No.: 221354-43-4
• Molecular Formula: C₁₄H₁₉NO₂S
• Molecular Weight: 265.376

Synonyms:2-<4-methyl-2-(methoxy)phenyl>-1-tetrahydro-2H-1,4-oxazin-4-yl-1-ethanthione

Chemical Property of 2-<4-methyl-2-(methoxy)phenyl>-1-tetrahydro-2H-1,4-oxazin-4-yl-1-ethanthione

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Technology Process of 2-<4-methyl-2-(methoxy)phenyl>-1-tetrahydro-2H-1,4-oxazin-4-yl-1-ethanthione

There total 5 articles about 2-<4-methyl-2-(methoxy)phenyl>-1-tetrahydro-2H-1,4-oxazin-4-yl-1-ethanthione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

morpholine (110-91-8,99108-56-2) + 2-methoxy-4-methylacetophenone (35633-35-3) → 2-<4-methyl-2-(methoxy)phenyl>-1-tetrahydro-2H-1,4-oxazin-4-yl-1-ethanthione (221354-43-4)

Guidance literature:

With sulfur; at 100 ℃; for 24h;

DOI:10.1016/S0040-4039(99)00768-6

Reference yield: 57.0%

morpholine (110-91-8,99108-56-2) + 2-methoxy-4-methylacetophenone (35633-35-3) → 2-<4-methyl-2-(methoxy)phenyl>-1-tetrahydro-2H-1,4-oxazin-4-yl-1-ethanthione (221354-43-4) + 1-<4-methyl-2-methoxyphenyl>-2--2-thioxo-1-ethanone (221354-65-0) + 3,4-di-<4-methyl-2-methoxyphenyl>-thiophene

Guidance literature:

With sulfur; at 100 - 120 ℃; for 24h;

DOI:10.1016/S0040-4020(98)01096-5

Reference yield: 17.0%

morpholine (110-91-8,99108-56-2) + 2-methoxy-4-methylacetophenone (35633-35-3) → 2-<4-methyl-2-(methoxy)phenyl>-1-tetrahydro-2H-1,4-oxazin-4-yl-1-ethanthione (221354-43-4) + 1-<4-methyl-2-methoxyphenyl>-2--2-thioxo-1-ethanone (221354-65-0) + 2,5-bis-(2-methoxy-4-methyl-phenyl)-thiophene

Guidance literature:

With sulfur; at 100 ℃;

DOI:10.1016/S0040-4020(00)01055-3

upstream raw materials:

morpholine

2-methoxy-4-methylacetophenone

4'-hydroxy-2'-methylacetophenone

3-acetoxytoluene

Downstream raw materials:

methyl 2-<4-methyl-2-methoxyphenyl>ethanethioate

methyl 2-[4-methyl-2-(methyloxy)phenyl]-5-hexenethioate

3,6-dimethyl-3H-benzo[b]furan-2-one

methyl 2-(2-methoxy-4-methylphenyl)propanethiolate

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