3-benzyloxy-N-(4''-tert-butyl-benzyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide

Base Information

• Chemical Name: 3-benzyloxy-N-(4''-tert-butyl-benzyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide
• CAS No.: 415974-55-9
• Molecular Formula: C₃₆H₄₁NO₃
• Molecular Weight: 535.726

Synonyms:3-benzyloxy-N-(4''-tert-butyl-benzyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide

Chemical Property of 3-benzyloxy-N-(4''-tert-butyl-benzyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide

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Technology Process of 3-benzyloxy-N-(4''-tert-butyl-benzyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide

There total 2 articles about 3-benzyloxy-N-(4''-tert-butyl-benzyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3-benzyloxy-16,17-seco-estra-1,3,5(10)-triene-16,17-imide (415974-45-7) → 3-benzyloxy-N-(4''-tert-butyl-benzyl)-16,17-seco-estra-1,3,5(10)-triene-16,17-imide (415974-55-9)

Guidance literature:

3-benzyloxy-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide; With sodium hydride; In N,N-dimethyl-formamide;

4-tert-butylbenzyl halide; In N,N-dimethyl-formamide;

DOI:10.1016/S0968-0896(03)00042-7

Reference yield:

3-benzyloxy-16,17-seco-estra-1,3,5(10)-triene-16,17-dioic acid (415974-44-6) → 3-benzyloxy-N-(4''-tert-butyl-benzyl)-16,17-seco-estra-1,3,5(10)-triene-16,17-imide (415974-55-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 89 percent / urea / 0.75 h / 180 °C

2.1: NaH / dimethylformamide

2.2: 97 percent / dimethylformamide

With sodium hydride; urea; In N,N-dimethyl-formamide;

DOI:10.1016/S0968-0896(03)00042-7

Reference yield: 87.0%

3-benzyloxy-N-(4''-tert-butyl-benzyl)-16,17-seco-estra-1,3,5(10)-triene-16,17-imide (415974-55-9) → 3-hydroxy-N-(4''-tert-butyl-benzyl)-16,17-seco-estra-1,3,5(10)-triene-16,17-imide (415974-65-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;

DOI:10.1016/S0968-0896(03)00042-7

upstream raw materials:

3-benzyloxy-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide

3-benzyloxy-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-dioic acid

Downstream raw materials:

3-hydroxy-N-(4''-tert-butyl-benzyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide

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