2-phenyldibenzo<1,3>dithiepin

Base Information

Chemical Name:2-phenyldibenzo<1,3>dithiepin
CAS No.:35864-05-2
Molecular Formula:C₁₉H₁₄S₂
Molecular Weight:306.452
Hs Code.:

Synonyms:2-phenyldibenzo<1,3>dithiepin

Suppliers and Price of 2-phenyldibenzo<1,3>dithiepin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-phenyldibenzo<1,3>dithiepin

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Technology Process of 2-phenyldibenzo<1,3>dithiepin

There total 2 articles about 2-phenyldibenzo<1,3>dithiepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 43216-01-9
2,2'-dimercaptobiphenyl

: 100-52-7
benzaldehyde

: 35864-05-2
2-phenyldibenzo<1,3>dithiepin

Guidance literature:: With tetrachlorosilane; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(99)00201-X

Reference yield:

: 230-26-2
dibenzo[1,2]dithiine

: 35864-05-2
2-phenyldibenzo<1,3>dithiepin

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / ethanol; tetrahydrofuran / Ambient temperature

2: 75 percent / SiCl₄ / CH₂Cl₂ / 2 h / Ambient temperature

With sodium tetrahydroborate; tetrachlorosilane; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/S0040-4020(99)00201-X