1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(carbamoylmethyl)-1,4,7,10-tetraazacyclododecane

Base Information

Chemical Name:1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(carbamoylmethyl)-1,4,7,10-tetraazacyclododecane
CAS No.:1073314-30-3
Molecular Formula:C₂₆H₄₆N₈O₃
Molecular Weight:518.703
Hs Code.:

Synonyms:1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(carbamoylmethyl)-1,4,7,10-tetraazacyclododecane

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Chemical Property of 1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(carbamoylmethyl)-1,4,7,10-tetraazacyclododecane

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Technology Process of 1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(carbamoylmethyl)-1,4,7,10-tetraazacyclododecane

There total 1 articles about 1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(carbamoylmethyl)-1,4,7,10-tetraazacyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 683-57-8
bromo-acetic acid amide

: 1073314-32-5
1-[3'-(N,N-diethylaminomethyl)benzyl]-1,4,7,10-tetraazacyclododecane

: 1073314-30-3
1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(carbamoylmethyl)-1,4,7,10-tetraazacyclododecane

Guidance literature:: With potassium carbonate; In ethanol; for 4h; Reflux;
DOI:10.1021/ja8037799

Reference yield: 90.0%

: 67-66-3,8013-54-5
chloroform

: 1073314-30-3
1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(carbamoylmethyl)-1,4,7,10-tetraazacyclododecane

: 52093-25-1
europium(III) trifluoromethanesulfonate

: [Eu(1-[3'-(N,N-diethylaminomethyl)benzyl]-4,7,10-tris(carbamoylmethyl)-1,4,7,10-tetraazacyclododecane)](CF₃SO₃)3*3CHCl₃*H₂O

Guidance literature:: In methanol; soln. Eu(CF3SO3)3 and ligandin dry MeOH was refluxed for 8 h; soln. was concd., CHCl3 was added, ppt. was dried in vacuo; elem. anal.;
DOI:10.1021/ja8037799