Technology Process of C17H23NO5SSi
There total 7 articles about C17H23NO5SSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
trimethylsilyl trifluoromethanesulfonate; C14H15NO5S;
With
triethylamine;
In
dichloromethane;
at 20 ℃;
for 1.5h;
Inert atmosphere;
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
dichloromethane;
at 20 ℃;
for 6h;
Inert atmosphere;
DOI:10.1021/ol201236j
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere
2.1: tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere
3.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C / Inert atmosphere
4.1: triethylamine / dichloromethane / 1.5 h / 20 °C / Inert atmosphere
4.2: 6 h / 20 °C / Inert atmosphere
With
sodium hydride; sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/ol201236j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere
2.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C / Inert atmosphere
3.1: triethylamine / dichloromethane / 1.5 h / 20 °C / Inert atmosphere
3.2: 6 h / 20 °C / Inert atmosphere
With
sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/ol201236j
