1-benzyl-3-cyano-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

Base Information

Chemical Name:1-benzyl-3-cyano-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide
CAS No.:1620644-77-0
Molecular Formula:C₂₅H₂₃N₂O₃*I
Molecular Weight:526.374
Hs Code.:

Synonyms:1-benzyl-3-cyano-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

Suppliers and Price of 1-benzyl-3-cyano-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-benzyl-3-cyano-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-benzyl-3-cyano-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

There total 6 articles about 1-benzyl-3-cyano-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1620646-03-8
4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylnicotinonitrile

: 100-39-0
benzyl bromide

: 1620644-77-0
1-benzyl-3-cyano-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

Guidance literature:: With sodium iodide; In dichloromethane; for 18h; Reflux;

Reference yield:

: 1332702-61-0
allyl 5,6-dimethoxy-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

: 1620644-77-0
1-benzyl-3-cyano-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; sodium iodide / acetone / 3 h / Reflux

2: triphenylphosphine; palladium diacetate; formic acid; triethylamine / tetrahydrofuran / 2.5 h / 20 - 70 °C / Inert atmosphere

3: sodium iodide / dichloromethane / 18 h / Reflux

With formic acid; palladium diacetate; potassium carbonate; triethylamine; triphenylphosphine; sodium iodide; In tetrahydrofuran; dichloromethane; acetone;

Reference yield:

: 1620646-02-7
allyl 2-(3-cyanopyridin-4-yl)methyl-5,6-dimethoxy-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

: 1620644-77-0
1-benzyl-3-cyano-4-(5,6-dimethoxy-1-oxo-2,3-dihydro-1H-inden-2-yl)methylpyridinium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; palladium diacetate; formic acid; triethylamine / tetrahydrofuran / 2.5 h / 20 - 70 °C / Inert atmosphere

2: sodium iodide / dichloromethane / 18 h / Reflux

With formic acid; palladium diacetate; triethylamine; triphenylphosphine; sodium iodide; In tetrahydrofuran; dichloromethane;