2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl 2-pyridinecarboxylate

Base Information

Chemical Name:2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl 2-pyridinecarboxylate
CAS No.:213819-56-8
Molecular Formula:C₃₃H₃₂N₄O₆
Molecular Weight:580.64
Hs Code.:

Synonyms:2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl 2-pyridinecarboxylate

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Chemical Property of 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl 2-pyridinecarboxylate

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Technology Process of 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl 2-pyridinecarboxylate

There total 1 articles about 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl 2-pyridinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 39901-94-5
2-picolinoyl chloride hydrochloride

: 2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-glucopyranose

: 213819-56-8
2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl 2-pyridinecarboxylate

Guidance literature:: With triethylamine; In dichloromethane; for 15h; Ambient temperature;
DOI:10.1248/cpb.46.1244

Reference yield:

: 53008-65-4,641635-63-4
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside

: 213819-56-8
2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl 2-pyridinecarboxylate

: methyl (3,4,6-tri-O-benzyl-2-azido-2-deoxy-β-D-glucopyranosyl)-(1→6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: methyl (3,4,6-tri-O-benzyl-2-azido-2-deoxy-α-D-glucopyranosyl)-(1→6)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With tin(II) trifluoromethanesulfonate; 4 A molecular sieve; In acetonitrile; at -30 - 20 ℃; for 2.5h; Yield given; Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1248/cpb.46.1244

Reference yield:

: 19488-48-3
methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 213819-56-8
2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl 2-pyridinecarboxylate

: methyl 2-azido-3,4,5-tri-O-benzyl-2-deoxy-D-glucopyranosyl-β-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: methyl 3,4,6-tri-O-benzyl-2-deoxy-2-azido-α-D-glucopyranosyl-(1→4)-2,3,4-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With tin(II) trifluoromethanesulfonate; 4 A molecular sieve; In acetonitrile; at -30 - 20 ℃; for 2.5h; Yield given; Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1248/cpb.46.1244