3,6-anhydro-1-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-glycero-D-talo/galacto octitol

Base Information

Chemical Name:3,6-anhydro-1-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-glycero-D-talo/galacto octitol
CAS No.:281666-27-1
Molecular Formula:C₁₈H₂₆O₆
Molecular Weight:338.401
Hs Code.:

Synonyms:3,6-anhydro-1-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-glycero-D-talo/galacto octitol

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Chemical Property of 3,6-anhydro-1-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-glycero-D-talo/galacto octitol

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Technology Process of 3,6-anhydro-1-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-glycero-D-talo/galacto octitol

There total 5 articles about 3,6-anhydro-1-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-glycero-D-talo/galacto octitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 281666-25-9
3,6-anhydro-1-O-benzyl-2-deoxy-4,5:7,8-di-O-isopropylidene-D-glycero-D-talo/galacto octitol

: 281666-27-1
3,6-anhydro-1-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-glycero-D-talo/galacto octitol

Guidance literature:: With acetic acid; at 20 ℃; for 7h;
DOI:10.1016/S0040-4020(00)00099-5

Reference yield:

: 100-39-0
benzyl bromide

: 281666-27-1
3,6-anhydro-1-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-glycero-D-talo/galacto octitol

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaH / dimethylformamide / 1 h / 20 °C

2: 85 percent / aq. AcOH / 7 h / 20 °C

With sodium hydride; acetic acid; In N,N-dimethyl-formamide; 1: Etherification / 2: Hydrolysis;
DOI:10.1016/S0040-4020(00)00099-5

Reference yield:

: 14131-84-1
2,3:5,6-di-O-isopropylidene-α-D-mannofuranose

: 281666-27-1
3,6-anhydro-1-O-benzyl-2-deoxy-4,5-O-isopropylidene-D-glycero-D-talo/galacto octitol

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / acetonitrile / 6 h / Heating

2: 0.63 g / LiAlH₄ / diethyl ether / 3 h / Heating

3: 94 percent / NaH / dimethylformamide / 1 h / 20 °C

4: 85 percent / aq. AcOH / 7 h / 20 °C

With lithium aluminium tetrahydride; sodium hydride; acetic acid; In diethyl ether; N,N-dimethyl-formamide; acetonitrile; 1: Substitution / 2: Reduction / 3: Etherification / 4: Hydrolysis;
DOI:10.1016/S0040-4020(00)00099-5