2-oxo-1-trityl-1,2-dihydropyrimidin-4-yl 2,4,6-triisopropylbenzenesulfonate

Base Information

Chemical Name:2-oxo-1-trityl-1,2-dihydropyrimidin-4-yl 2,4,6-triisopropylbenzenesulfonate
CAS No.:1243253-29-3
Molecular Formula:C₃₈H₄₀N₂O₄S
Molecular Weight:620.813
Hs Code.:

Synonyms:2-oxo-1-trityl-1,2-dihydropyrimidin-4-yl 2,4,6-triisopropylbenzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-oxo-1-trityl-1,2-dihydropyrimidin-4-yl 2,4,6-triisopropylbenzenesulfonate

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Technology Process of 2-oxo-1-trityl-1,2-dihydropyrimidin-4-yl 2,4,6-triisopropylbenzenesulfonate

There total 1 articles about 2-oxo-1-trityl-1,2-dihydropyrimidin-4-yl 2,4,6-triisopropylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 1243253-55-5
1-tritylpyrimidine-2,4(1H,3H)-dione

: 1243253-29-3
2-oxo-1-trityl-1,2-dihydropyrimidin-4-yl 2,4,6-triisopropylbenzenesulfonate

Guidance literature:: 1-tritylpyrimidine-2,4(1H,3H)-dione; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.75h;

2,4,6-triisopropylphenylsulfonyl chloride; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 1243253-29-3
2-oxo-1-trityl-1,2-dihydropyrimidin-4-yl 2,4,6-triisopropylbenzenesulfonate

: 154230-29-2
(E)-4-chlorostyrylboronic acid

: 1243253-33-9
4-[2-(4-chlorophenyl)ethenyl]-1H-pyrimidine-2-one

Guidance literature:: 2-oxo-1-trityl-1,2-dihydropyrimidin-4-yl 2,4,6-triisopropylbenzenesulfonate; (E)-4-chlorostyrylboronic acid; With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 48 ℃; for 14h;

With methanol; Sonication;