methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-formamido-β-D-glucopyranosyl)-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-formamido-β-D-glucopyranosyl)-α-D-glucopyranoside
CAS No.:125084-93-7
Molecular Formula:C₄₁H₄₉NO₁₄
Molecular Weight:779.838
Hs Code.:

Synonyms:methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-formamido-β-D-glucopyranosyl)-α-D-glucopyranoside

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Chemical Property of methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-formamido-β-D-glucopyranosyl)-α-D-glucopyranoside

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Technology Process of methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-formamido-β-D-glucopyranosyl)-α-D-glucopyranoside

There total 3 articles about methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-formamido-β-D-glucopyranosyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 76695-53-9
1,3,4,6-Tetra-O-acetyl-2-desoxy-2-formamido-β-D-glucose

: 19488-48-3
methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 125084-93-7
methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-formamido-β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 Angstroem MS; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4039(01)80443-3

Reference yield: 15.0%

: 19488-48-3
methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 125084-87-9
3,4,6-tri-O-acetyl-2-deoxy-2-formamido-α-D-glucopyranosyl chloride

: 125084-93-7
methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-formamido-β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: With 4 Angstroem MS; silver trifluoromethanesulfonate; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4039(01)80443-3

Reference yield:

: 76695-53-9
1,3,4,6-Tetra-O-acetyl-2-desoxy-2-formamido-β-D-glucose

: 125084-93-7
methyl 2,3,6-tri-O-benzyl-4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-formamido-β-D-glucopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / HCl, / various solvent(s) / 1.) 0 deg C, 2.) RT; overnight,

2: 15 percent / silver triflate, molecular sieves 4A, / CH₂Cl₂ / Ambient temperature

With hydrogenchloride; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1016/0008-6215(89)85044-X