Methyl-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Base Information

Chemical Name:Methyl-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid
CAS No.:112622-76-1
Molecular Formula:C₆₉H₇₆N₄O₁₆
Molecular Weight:1217.38
Hs Code.:

Methyl-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Synonyms:Methyl-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

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Chemical Property of Methyl-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

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Technology Process of Methyl-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

There total 8 articles about Methyl-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 112622-75-0
Methyl-O-(6-O-acetyl-2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-(1->4)-O-(2-O-acetyl-3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

: 112622-76-1
Methyl-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Guidance literature:: With sodium methylate; In methanol; for 10h;

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 112622-76-1
Methyl-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / p-toluenesulfonic acid / dimethylformamide / 3 h / 60 °C

2: 92 percent / pyridine

3: 92 percent / NaBH₃CN, HCl, molecular sieve / tetrahydrofuran; diethyl ether / 0 °C

4: 92 percent / CF₃SO₃Ag, collidine, molecular sieve / CH₂Cl₂ / 6 h / -50 - -30 °C

5: 77 percent / 1 N CH₃ONa / methanol / 10 h

With pyridine; 2,3,5-trimethyl-pyridine; hydrogenchloride; molecular sieve; sodium methylate; silver trifluoromethanesulfonate; sodium cyanoborohydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 110236-58-3
Methyl-3,6-di-O-benzyl-4-O-(3-O-benzyl-α-L-idopyranosyl)-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

: 112622-76-1
Methyl-O-(2-azido-3,4-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)-(1->4)-O-(3,6-di-O-benzyl-α-L-idopyranosyl)-(1->4)-3,6-di-O-benzyl-2-(benzyloxycarbonylamino)-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / p-toluenesulfonic acid / dimethylformamide / 3 h / 60 °C

2: 92 percent / pyridine

3: 92 percent / NaBH₃CN, HCl, molecular sieve / tetrahydrofuran; diethyl ether / 0 °C

4: 92 percent / CF₃SO₃Ag, collidine, molecular sieve / CH₂Cl₂ / 6 h / -50 - -30 °C

5: 77 percent / 1 N CH₃ONa / methanol / 10 h

With pyridine; 2,3,5-trimethyl-pyridine; hydrogenchloride; molecular sieve; sodium methylate; silver trifluoromethanesulfonate; sodium cyanoborohydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;