(Ir(NC₅H₄(CH₂)2P(C₆H₅)2)(C₈H₁₂))⁽¹⁺⁾*PF₆^(1-)=(Ir(NC₅H₄(CH₂)2P(C₆H₅)2)(C₈H₁₂))PF₆

Base Information

• Chemical Name: (Ir(NC₅H₄(CH₂)2P(C₆H₅)2)(C₈H₁₂))⁽¹⁺⁾*PF₆^(1-)=(Ir(NC₅H₄(CH₂)2P(C₆H₅)2)(C₈H₁₂))PF₆
• CAS No.: 112021-45-1
• Molecular Formula: C₂₇H₃₀IrNP*F₆P
• Molecular Weight: 736.7

Synonyms:(Ir(NC₅H₄(CH₂)2P(C₆H₅)2)(C₈H₁₂))⁽¹⁺⁾*PF₆^(1-)=(Ir(NC₅H₄(CH₂)2P(C₆H₅)2)(C₈H₁₂))PF₆

Chemical Property of (Ir(NC₅H₄(CH₂)2P(C₆H₅)2)(C₈H₁₂))⁽¹⁺⁾*PF₆^(1-)=(Ir(NC₅H₄(CH₂)2P(C₆H₅)2)(C₈H₁₂))PF₆

Chemical Property:

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Technology Process of (Ir(NC₅H₄(CH₂)2P(C₆H₅)2)(C₈H₁₂))⁽¹⁺⁾*PF₆^(1-)=(Ir(NC₅H₄(CH₂)2P(C₆H₅)2)(C₈H₁₂))PF₆

There total 1 articles about (Ir(NC₅H₄(CH₂)2P(C₆H₅)2)(C₈H₁₂))⁽¹⁺⁾*PF₆^(1-)=(Ir(NC₅H₄(CH₂)2P(C₆H₅)2)(C₈H₁₂))PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

chloro(1,5-cyclooctadiene)iridium(I) dimer + 2-(2-(diphenylphosphino)ethyl)pyridine (10150-27-3) → (Ir(NC5H4(CH2)2P(C6H5)2)(C8H12))(1+)*PF6(1-)=(Ir(NC5H4(CH2)2P(C6H5)2)(C8H12))PF6 (112021-45-1)

Guidance literature:

With AgPF₆; In isopropyl alcohol; acetone; byproducts: AgCl; N2-atmosphere, stirring for 15 min, filtn. over diatomceous earth, addn. of PN-ligand in isopropyl alcohol, stirring for 15 min.; Crystn. by concn., recrystn. from acetone/Et2O, elem. anal.;

Reference yield: 80.0%

(Ir(NC5H4(CH2)2P(C6H5)2)(C8H12))(1+)*PF6(1-)=(Ir(NC5H4(CH2)2P(C6H5)2)(C8H12))PF6 (112021-45-1) → (Ir3(NC5H4(CH2)2P(C6H5)2)3(H)7)(2+)*2PF6(1-)=(Ir3(NC5H4(CH2)2P(C6H5)2)3(H)7)(PF6)2 (112021-47-3)

Guidance literature:

With H₂; In methanol; N2-atmosphere, stirring under 1 atm H2 for 2 h.; Filtration, washing with Et2O, elem. anal.;

Reference yield: 76.0%

{iridium(1-(2-pyridyl)-2-(diphenylphosphino)ethane)(1,5-cyclooctadiene)}PF6 (112021-45-1) + 2-(2-(diphenylphosphino)ethyl)pyridine (10150-27-3) → {iridium(1-(2-pyridyl)-2-(diphenylphosphino)ethane)2}PF6*0.45CH2Cl2 (113705-90-1)

Guidance literature:

In acetone; Under N2, a red-orange soln. of {Ir(PN)(cod)}PF6 is added to excess PN, the soln. is stirred at 50°C for 30 min, color fades to a light orange.; Layering the soln. with Et2O, recrystn. from CH2Cl2/Et2O, elem. anal.;

upstream raw materials:

2-(2-(diphenylphosphino)ethyl)pyridine

Downstream raw materials:

{iridium(1-(2-pyridyl)-2-(diphenylphosphino)ethane)2}PF₆*0.45CH₂Cl₂

(Ir₃(NC₅H₄(CH₂)2P(C₆H₅)2)3(D)7)⁽²⁺⁾*2PF₆^(1-)=(Ir₃(NC₅H₄(CH₂)2P(C₆H₅)2)3(D)7)(PF₆)2

(Ir₃(NC₅H₄(CH₂)2P(C₆H₅)2)3(H)7)⁽²⁺⁾*2PF₆^(1-)=(Ir₃(NC₅H₄(CH₂)2P(C₆H₅)2)3(H)7)(PF₆)2

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