IrBr(CO)(P(C₆H₅)3)2(SC(CN)C(CN)S)

Base Information

Chemical Name:IrBr(CO)(P(C₆H₅)3)2(SC(CN)C(CN)S)
CAS No.:120156-95-8
Molecular Formula:C₄₁H₃₀BrIrN₂OP₂S₂
Molecular Weight:964.906
Hs Code.:

IrBr(CO)(P(C<sub>6</sub>H<sub>5</sub>)3)2(SC(CN)C(CN)S)

Synonyms:IrBr(CO)(P(C₆H₅)3)2(SC(CN)C(CN)S)

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Chemical Property of IrBr(CO)(P(C₆H₅)3)2(SC(CN)C(CN)S)

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Technology Process of IrBr(CO)(P(C₆H₅)3)2(SC(CN)C(CN)S)

There total 3 articles about IrBr(CO)(P(C₆H₅)3)2(SC(CN)C(CN)S) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 84623-89-2
(tetra-n-butylammonium){Ir(CO)(PPh₃)(maleonitriledithiolate)}

: 120156-95-8
IrBr(CO)(P(C₆H₅)3)2(SC(CN)C(CN)S)

Guidance literature:: With Br₂; triphenyl phosphine; In acetone; under N2; to a soln. of the Ir complex in acetone was added Br2, stirred for 2 h, addn. of an acetone soln. of PPh3, stirred for 30 min; concd., addn. of 2-propanol, concd., stored at -20°C overnight, filtered, washed with hexanes; elem. anal.;
DOI:10.1021/ja00086a019

Reference yield:

: (CO)(CH₃)Ir((P(C₆H₅)3))2(S₂C₄N₂)

: 2909-52-6
tribromo(2H)methane

: 120156-95-8
IrBr(CO)(P(C₆H₅)3)2(SC(CN)C(CN)S)

Guidance literature:: In further solvent(s); byproducts: CH3Br; Irradiation (UV/VIS); under N2; in CDBr3; identified by NMR;
DOI:10.1021/ja00086a019

Reference yield:

: (CO)(CH₃)Ir((P(C₆H₅)3))2(S₂C₄N₂)

: 120156-95-8
IrBr(CO)((P(C₆H₅)3))2(S₂C₄N₂)

Guidance literature:: With CDBr₃; In benzene; byproducts: CH3Br; Irradiation (UV/VIS); photolysis (medium pressure Hg arc lamp, 350-500 nm bandpass filter, 55 h), ca. 50 equiv. CDBr3;
DOI:10.1039/c39880000255