C₂₆H₂₅NO₅

Base Information

Chemical Name:C₂₆H₂₅NO₅
CAS No.:1276098-91-9
Molecular Formula:C₂₆H₂₅NO₅
Molecular Weight:431.488
Hs Code.:

C<sub>26</sub>H<sub>25</sub>NO<sub>5</sub>

Synonyms:C₂₆H₂₅NO₅

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Chemical Property of C₂₆H₂₅NO₅

Chemical Property:

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Technology Process of C₂₆H₂₅NO₅

There total 4 articles about C₂₆H₂₅NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 86286-50-2
(4R,5S)-4,5-diphenyl-1,3-oxazolidin-2-one

: 51267-07-3
(2,5-dimethoxy-4-methyl-phenyl)-acetic acid

: 1276098-91-9
C₂₆H₂₅NO₅

Guidance literature:: (4R,5S)-4,5-diphenyl-1,3-oxazolidin-2-one; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; Inert atmosphere;

(2,5-dimethoxy-4-methyl-phenyl)-acetic acid; With pivaloyl chloride; triethylamine; In tetrahydrofuran; diethyl ether; hexane; at -78 - 0 ℃; Inert atmosphere;
DOI:10.1007/s11426-010-4173-y

Reference yield:

: 13321-74-9
1-bromo-2,5-dimethoxy-4-methylbenzene

: 1276098-91-9
C₂₆H₂₅NO₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere

1.2: 0.33 h / -78 °C / Inert atmosphere

1.3: Inert atmosphere

2.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0 - 20 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

4.2: -78 - 0 °C / Inert atmosphere

With sodium chlorite; n-butyllithium; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; hexane; dichloromethane; water; tert-butyl alcohol; 3.1: Pinnick oxidation;
DOI:10.1007/s11426-010-4173-y

Reference yield:

: 38439-76-8
2-(2,5-dimethoxy-4-methylphenyl)ethanol

: 1276098-91-9
C₂₆H₂₅NO₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

3.2: -78 - 0 °C / Inert atmosphere

With sodium chlorite; n-butyllithium; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; hexane; dichloromethane; water; tert-butyl alcohol; 2.1: Pinnick oxidation;
DOI:10.1007/s11426-010-4173-y