6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid

Base Information

Chemical Name:6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid
CAS No.:1258832-02-8
Molecular Formula:C₂₆H₂₇N₅O₅
Molecular Weight:489.531
Hs Code.:

Synonyms:6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid

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Chemical Property of 6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid

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Technology Process of 6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid

There total 1 articles about 6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1258832-20-0
6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid ethyl ester

: 1258832-02-8
6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid

Guidance literature:: 6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid ethyl ester; With potassium trimethylsilonate; In tetrahydrofuran; at 20 ℃; for 12h;

With water; In tetrahydrofuran; dichloromethane; at 0 ℃;

With citric acid; In tetrahydrofuran; dichloromethane; water; at 0 ℃; pH=6;
DOI:10.1002/chem.201001861

Reference yield: 96.0%

: 1258832-02-8
6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid

: 21761-30-8,76969-52-3
L-valyl-L-valine methyl ester

: 1258832-21-1
C₃₇H₄₇N₇O₇

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1002/chem.201001861

Reference yield: 90.0%

: 1258832-02-8
6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid

: 7517-19-3
methyl (L)-leucinate hydrochloride

: 1258832-23-3
C₃₃H₄₀N₆O₆

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1002/chem.201001861