6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid ethyl ester

Base Information

Chemical Name:6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid ethyl ester
CAS No.:1258832-20-0
Molecular Formula:C₂₈H₃₁N₅O₅
Molecular Weight:517.585
Hs Code.:

Synonyms:6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid ethyl ester

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Chemical Property of 6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid ethyl ester

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Technology Process of 6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid ethyl ester

There total 1 articles about 6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 944150-45-2
benzyl {[3-(benzylamino)-3-oxopropyl]amino}carbonothioyl carbamate

: 104086-21-7
6-(aminomethyl)pyridine-2-carboxylic acid ethyl ester

: 1258832-20-0
6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid ethyl ester

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1002/chem.201001861

Reference yield: 90.0%

: 1258832-20-0
6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid ethyl ester

: 1258832-02-8
6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid

Guidance literature:: 6-{[3-(3-(benzylamino)-3-oxopropyl)-2-((benzyloxy)carbonyl)guanidino]methyl}picolinic acid ethyl ester; With potassium trimethylsilonate; In tetrahydrofuran; at 20 ℃; for 12h;

With water; In tetrahydrofuran; dichloromethane; at 0 ℃;

With citric acid; In tetrahydrofuran; dichloromethane; water; at 0 ℃; pH=6;
DOI:10.1002/chem.201001861