Tungsten,pentacarbonyl(4-methylpyridine)-, (OC-6-22)-

Base Information

Chemical Name:Tungsten,pentacarbonyl(4-methylpyridine)-, (OC-6-22)-
CAS No.:17000-14-5
Molecular Formula:C11H7 N O5 W
Molecular Weight:417.03
Hs Code.:
Mol file:17000-14-5.mol

Synonyms:Tungsten,pentacarbonyl(4-picoline)- (8CI); Pentacarbonyl(4-picoline)tungsten

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Tungsten,pentacarbonyl(4-methylpyridine)-, (OC-6-22)-

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Technology Process of Tungsten,pentacarbonyl(4-methylpyridine)-, (OC-6-22)-

There total 1 articles about Tungsten,pentacarbonyl(4-methylpyridine)-, (OC-6-22)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-89-4
picoline

: 14780-97-3
tetraethylammonium chloropentacarbonyltungstate

: 14040-11-0
tungsten hexacarbonyl

: 84076-49-3
W(CO)4(4-methylpyridine)2

: 17000-14-5
pentacarbonyl-4-methylpyridine-tungsten⁽⁰⁾

Guidance literature:: In further solvent(s); in presence of NaBPh4, stirring in 4-methylpyridine for several h; pptn. on water addn., collection, sublimation off of W(CO)6 (vac., 50°C), extn. into hexane, recrystn. (hexane); elem. anal.;
DOI:10.1016/S0020-1693(00)91080-6