cis-8-allyl-6-(tert-butyl-diphenylsilanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

Base Information

Chemical Name:cis-8-allyl-6-(tert-butyl-diphenylsilanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine
CAS No.:1187063-41-7
Molecular Formula:C₃₀H₃₄N₄O₂Si
Molecular Weight:510.711
Hs Code.:

Synonyms:cis-8-allyl-6-(tert-butyl-diphenylsilanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

Suppliers and Price of cis-8-allyl-6-(tert-butyl-diphenylsilanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of cis-8-allyl-6-(tert-butyl-diphenylsilanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of cis-8-allyl-6-(tert-butyl-diphenylsilanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

There total 2 articles about cis-8-allyl-6-(tert-butyl-diphenylsilanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: C₂₇H₃₀N₄O₂Si

: 106-95-6
allyl bromide

: 1187063-41-7
cis-8-allyl-6-(tert-butyl-diphenylsilanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

: 1187063-36-0
(6R,8S)-8-allyl-6-(((tert-butyldiphenylsilyl)oxy)methyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/acs.orglett.9b01842

Reference yield:

: 556-56-9
allyl iodid

: 1187063-28-0
cis-6-(tert-butyl-diphenyl-silanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

: 1187063-41-7
cis-8-allyl-6-(tert-butyl-diphenylsilanyloxymethyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

: 1187063-36-0
(6R,8S)-8-allyl-6-(((tert-butyldiphenylsilyl)oxy)methyl)-8-phenyl-5,6-dihydro-8H-tetrazolo[5,1-c][1,4]oxazine

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -100 ℃; for 4h; optical yield given as %de; diastereoselective reaction;
DOI:10.1016/j.tet.2009.06.033