7-(o-formyl)phenylaminophthalide

Base Information

Chemical Name:7-(o-formyl)phenylaminophthalide
CAS No.:327626-91-5
Molecular Formula:C₁₅H₁₁NO₃
Molecular Weight:253.257
Hs Code.:

Synonyms:7-(o-formyl)phenylaminophthalide

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Chemical Property of 7-(o-formyl)phenylaminophthalide

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Technology Process of 7-(o-formyl)phenylaminophthalide

There total 4 articles about 7-(o-formyl)phenylaminophthalide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 327626-90-4
7-(o-hydroxymethyl)phenylaminophthalide

: 327626-91-5
7-(o-formyl)phenylaminophthalide

Guidance literature:: With manganese(IV) oxide; In acetone; at 20 ℃; for 96h;
DOI:10.1021/jo000118y

Reference yield:

: 3883-64-5
7-aminophthalide

: 327626-91-5
7-(o-formyl)phenylaminophthalide

Guidance literature:: Multi-step reaction with 3 steps

1.1: cupric acetate / propan-2-ol / 24 h / Heating

2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 24 h / 20 °C

2.2: 78 percent / NaBH₄ / tetrahydrofuran; H₂O / 0.33 h / 20 °C

3.1: 94 percent / MnO₂ / acetone / 96 h / 20 °C

With manganese(IV) oxide; copper diacetate; 1,1'-carbonyldiimidazole; In tetrahydrofuran; isopropyl alcohol; acetone;
DOI:10.1021/jo000118y

Reference yield:

: 1488-42-2,109545-72-4
Diphenyliodonium-2-carboxylate

: 327626-91-5
7-(o-formyl)phenylaminophthalide

Guidance literature:: Multi-step reaction with 3 steps

1.1: cupric acetate / propan-2-ol / 24 h / Heating

2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 24 h / 20 °C

2.2: 78 percent / NaBH₄ / tetrahydrofuran; H₂O / 0.33 h / 20 °C

3.1: 94 percent / MnO₂ / acetone / 96 h / 20 °C

With manganese(IV) oxide; copper diacetate; 1,1'-carbonyldiimidazole; In tetrahydrofuran; isopropyl alcohol; acetone;
DOI:10.1021/jo000118y