(E)-6-amino-3-(4-(dimethylamino)benzylidene)-2,3-dihydropyrrolo[2,1-b]quinazolin-9(1H)-one

Base Information

Chemical Name:(E)-6-amino-3-(4-(dimethylamino)benzylidene)-2,3-dihydropyrrolo[2,1-b]quinazolin-9(1H)-one
CAS No.:1337863-27-0
Molecular Formula:C₂₀H₂₀N₄O
Molecular Weight:332.405
Hs Code.:

Synonyms:(E)-6-amino-3-(4-(dimethylamino)benzylidene)-2,3-dihydropyrrolo[2,1-b]quinazolin-9(1H)-one

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Chemical Property of (E)-6-amino-3-(4-(dimethylamino)benzylidene)-2,3-dihydropyrrolo[2,1-b]quinazolin-9(1H)-one

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Technology Process of (E)-6-amino-3-(4-(dimethylamino)benzylidene)-2,3-dihydropyrrolo[2,1-b]quinazolin-9(1H)-one

There total 3 articles about (E)-6-amino-3-(4-(dimethylamino)benzylidene)-2,3-dihydropyrrolo[2,1-b]quinazolin-9(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1337863-20-3
(E)-3-(4-(dimethylamino)benzylidene)-6-nitro-2,3-dihydropyrrolo[2,1-b]quinazolin-9(1H)-one

: 1337863-27-0
(E)-6-amino-3-(4-(dimethylamino)benzylidene)-2,3-dihydropyrrolo[2,1-b]quinazolin-9(1H)-one

Guidance literature:: With sodiumsulfide nonahydrate; sodium hydroxide; In ethanol; water; for 6h; Reflux;
DOI:10.1039/c1ob05884c

Reference yield:

: 619-17-0
4-Nitroanthranilic acid

: 1337863-27-0
(E)-6-amino-3-(4-(dimethylamino)benzylidene)-2,3-dihydropyrrolo[2,1-b]quinazolin-9(1H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / toluene / Reflux

2: sodium acetate; acetic acid / 8 h / Reflux

3: sodiumsulfide nonahydrate; sodium hydroxide / ethanol; water / 6 h / Reflux

With sodiumsulfide nonahydrate; sodium acetate; acetic acid; sodium hydroxide; trichlorophosphate; In ethanol; water; toluene;
DOI:10.1039/c1ob05884c

Reference yield:

: 55727-50-9
6-nitro-2,3-dihydropyrrolo[2,1-b]quinazolin-9(1H)-one

: 1337863-27-0
(E)-6-amino-3-(4-(dimethylamino)benzylidene)-2,3-dihydropyrrolo[2,1-b]quinazolin-9(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate; acetic acid / 8 h / Reflux

2: sodiumsulfide nonahydrate; sodium hydroxide / ethanol; water / 6 h / Reflux

With sodiumsulfide nonahydrate; sodium acetate; acetic acid; sodium hydroxide; In ethanol; water;
DOI:10.1039/c1ob05884c