1-[1-(3,5-dimethoxybenzyl)-1H-1,2,3-triazol-4-yl]-2-phenylethane-1,2-dione

Base Information

Chemical Name:1-[1-(3,5-dimethoxybenzyl)-1H-1,2,3-triazol-4-yl]-2-phenylethane-1,2-dione
CAS No.:1357356-76-3
Molecular Formula:C₁₉H₁₇N₃O₄
Molecular Weight:351.362
Hs Code.:

Synonyms:1-[1-(3,5-dimethoxybenzyl)-1H-1,2,3-triazol-4-yl]-2-phenylethane-1,2-dione

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Chemical Property of 1-[1-(3,5-dimethoxybenzyl)-1H-1,2,3-triazol-4-yl]-2-phenylethane-1,2-dione

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Technology Process of 1-[1-(3,5-dimethoxybenzyl)-1H-1,2,3-triazol-4-yl]-2-phenylethane-1,2-dione

There total 4 articles about 1-[1-(3,5-dimethoxybenzyl)-1H-1,2,3-triazol-4-yl]-2-phenylethane-1,2-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1345823-27-9
1-(1-(3,5-dimethoxybenzyl)-1H-1,2,3-triazol-4-yl)-2-phenylethanone

: 1357356-76-3
1-[1-(3,5-dimethoxybenzyl)-1H-1,2,3-triazol-4-yl]-2-phenylethane-1,2-dione

Guidance literature:: With copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; In acetonitrile; at 80 ℃;
DOI:10.1002/ejoc.201101346

Reference yield:

: 88768-84-7
1-phenyl-4-trimethylsilylbutane-3-yn-2-one

: 712329-47-0
1-(azidomethyl)-3,5-dimethoxybenzene

: 1357356-76-3
1-[1-(3,5-dimethoxybenzyl)-1H-1,2,3-triazol-4-yl]-2-phenylethane-1,2-dione

Guidance literature:: 1-phenyl-4-trimethylsilylbutane-3-yn-2-one; 1-(azidomethyl)-3,5-dimethoxybenzene; With water; sodium L-ascorbate; copper dichloride; In acetonitrile; at 80 ℃; for 1h;

With 2.9-dimethyl-1,10-phenanthroline; In acetonitrile; at 80 ℃; for 20h;
DOI:10.1016/j.ejmech.2013.06.042

Reference yield:

: 103-80-0
phenylacetyl chloride

: 1357356-76-3
1-[1-(3,5-dimethoxybenzyl)-1H-1,2,3-triazol-4-yl]-2-phenylethane-1,2-dione

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / dichloromethane / 0 °C

2: sodium L-ascorbate; copper dichloride / water; acetonitrile / 20 - 80 °C

3: copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline / acetonitrile / 80 °C

With aluminum (III) chloride; copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; sodium L-ascorbate; copper dichloride; In dichloromethane; water; acetonitrile;
DOI:10.1002/ejoc.201101346