dibutyl (4-methoxy-2-(5-(trifluoromethyl)pyridin-2-yl)phenyl)phosphonate

Base Information

Chemical Name:dibutyl (4-methoxy-2-(5-(trifluoromethyl)pyridin-2-yl)phenyl)phosphonate
CAS No.:1459258-96-8
Molecular Formula:C₂₁H₂₇F₃NO₄P
Molecular Weight:445.419
Hs Code.:

Synonyms:dibutyl (4-methoxy-2-(5-(trifluoromethyl)pyridin-2-yl)phenyl)phosphonate

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Chemical Property of dibutyl (4-methoxy-2-(5-(trifluoromethyl)pyridin-2-yl)phenyl)phosphonate

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Technology Process of dibutyl (4-methoxy-2-(5-(trifluoromethyl)pyridin-2-yl)phenyl)phosphonate

There total 2 articles about dibutyl (4-methoxy-2-(5-(trifluoromethyl)pyridin-2-yl)phenyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 370878-65-2
2-(3-methoxyphenyl)-5-(trifluoromethyl)pyridine

: 109632-36-2
dibutyl (2-hydroxypropan-2-yl)phosphonate

: 1459258-96-8
dibutyl (4-methoxy-2-(5-(trifluoromethyl)pyridin-2-yl)phenyl)phosphonate

Guidance literature:: With N-methylmaleimide; dipotassium hydrogenphosphate; silver(I) acetate; palladium diacetate; In tert-butyl alcohol; at 120 ℃; for 48h;
DOI:10.1002/anie.201305202

Reference yield:

: 1809-19-4
dibutyl hydrogen phosphite

: 1459258-96-8
dibutyl (4-methoxy-2-(5-(trifluoromethyl)pyridin-2-yl)phenyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium chloride; triethylamine / 40 °C

2: palladium diacetate; N-methylmaleimide; silver(I) acetate; dipotassium hydrogenphosphate / tert-butyl alcohol / 48 h / 120 °C

With N-methylmaleimide; dipotassium hydrogenphosphate; silver(I) acetate; palladium diacetate; triethylamine; magnesium chloride; In tert-butyl alcohol;
DOI:10.1002/anie.201305202