Benzyl-((Z)-(S)-1-methyl-4-trimethylsilanyl-but-3-enyl)-trimethylsilanylmethyl-amine

Base Information

Chemical Name:Benzyl-((Z)-(S)-1-methyl-4-trimethylsilanyl-but-3-enyl)-trimethylsilanylmethyl-amine
CAS No.:153682-00-9
Molecular Formula:C₁₉H₃₅NSi₂
Molecular Weight:333.665
Hs Code.:

Synonyms:Benzyl-((Z)-(S)-1-methyl-4-trimethylsilanyl-but-3-enyl)-trimethylsilanylmethyl-amine

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Chemical Property of Benzyl-((Z)-(S)-1-methyl-4-trimethylsilanyl-but-3-enyl)-trimethylsilanylmethyl-amine

Chemical Property:

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Technology Process of Benzyl-((Z)-(S)-1-methyl-4-trimethylsilanyl-but-3-enyl)-trimethylsilanylmethyl-amine

There total 4 articles about Benzyl-((Z)-(S)-1-methyl-4-trimethylsilanyl-but-3-enyl)-trimethylsilanylmethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 4206-67-1
iodo(trimethylsilyl)methane

: 153681-99-3
(S)-N-benzyl-N-(Z)-(1-methyl-4-trimethylsilylbut-3-enyl)amine

: 153682-00-9
Benzyl-((Z)-(S)-1-methyl-4-trimethylsilanyl-but-3-enyl)-trimethylsilanylmethyl-amine

Guidance literature:: With potassium carbonate; In acetonitrile; for 48h; Heating;
DOI:10.1021/jo971706n

Reference yield:

: 100-39-0
benzyl bromide

: 153682-00-9
Benzyl-((Z)-(S)-1-methyl-4-trimethylsilanyl-but-3-enyl)-trimethylsilanylmethyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / K₂CO₃ / dimethylformamide / 12 h / 25 °C

2: 80 percent / Na/Hg, Na₂HPO₄ / methanol / 12 h / Heating

3: 53 percent / K₂CO₃ / acetonitrile / 48 h / Heating

With disodium hydrogenphosphate; sodium amalgam; potassium carbonate; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo971706n

Reference yield:

: 119461-42-6
(S)-N-(p-toluenesulfonyl)-4-amino-1-Z-(trimethylsilyl)-1-pentene

: 153682-00-9
Benzyl-((Z)-(S)-1-methyl-4-trimethylsilanyl-but-3-enyl)-trimethylsilanylmethyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / K₂CO₃ / dimethylformamide / 12 h / 25 °C

2: 80 percent / Na/Hg, Na₂HPO₄ / methanol / 12 h / Heating

3: 53 percent / K₂CO₃ / acetonitrile / 48 h / Heating

With disodium hydrogenphosphate; sodium amalgam; potassium carbonate; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo971706n