C₃₅H₄₉NO₇S₂Si

Base Information

Chemical Name:C₃₅H₄₉NO₇S₂Si
CAS No.:1319713-20-6
Molecular Formula:C₃₅H₄₉NO₇S₂Si
Molecular Weight:687.994
Hs Code.:

C<sub>35</sub>H<sub>49</sub>NO<sub>7</sub>S<sub>2</sub>Si

Synonyms:C₃₅H₄₉NO₇S₂Si

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Chemical Property of C₃₅H₄₉NO₇S₂Si

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Technology Process of C₃₅H₄₉NO₇S₂Si

There total 6 articles about C₃₅H₄₉NO₇S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1319713-26-2
C₂₉H₄₅NO₅SSi

: 98-09-9
benzenesulfonyl chloride

: 1319713-20-6
C₃₅H₄₉NO₇S₂Si

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2011.05.091

Reference yield:

: 1319713-15-9
C₁₀H₁₃BrO₄

: 1319713-20-6
C₃₅H₄₉NO₇S₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere; Reflux

2.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 1.17 h / -78 - 20 °C / Inert atmosphere

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.2: 2 h / Inert atmosphere

4.1: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / Inert atmosphere; Reflux

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.83 h / 0 °C / Inert atmosphere

6.1: triethylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; oxalyl dichloride; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; dimethyl sulfoxide; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; toluene; 2.1: Swern oxidation / 3.1: Horner-Wadsworth-Emmons olefination;
DOI:10.1016/j.tetlet.2011.05.091

Reference yield:

: 1319713-16-0
C₁₉H₃₃BrO₄Si

: 1319713-20-6
C₃₅H₄₉NO₇S₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 1.17 h / -78 - 20 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 2 h / Inert atmosphere

3.1: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / Inert atmosphere; Reflux

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.83 h / 0 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; oxalyl dichloride; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; dimethyl sulfoxide; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; toluene; 1.1: Swern oxidation / 2.1: Horner-Wadsworth-Emmons olefination;
DOI:10.1016/j.tetlet.2011.05.091