4-benzyl-5-(3,4,5-trimethoxyphenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

Base Information

Chemical Name:4-benzyl-5-(3,4,5-trimethoxyphenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole
CAS No.:1430730-44-1
Molecular Formula:C₅₂H₄₅N₃O₁₂
Molecular Weight:903.942
Hs Code.:

Synonyms:4-benzyl-5-(3,4,5-trimethoxyphenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

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Chemical Property of 4-benzyl-5-(3,4,5-trimethoxyphenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

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Technology Process of 4-benzyl-5-(3,4,5-trimethoxyphenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

There total 4 articles about 4-benzyl-5-(3,4,5-trimethoxyphenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 706784-62-5
5-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)tetrazole

: C₁₇H₁₈ClNO₃

: 1430730-44-1
4-benzyl-5-(3,4,5-trimethoxyphenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

Guidance literature:: In m-xylene; for 8h; Reflux;

Reference yield:

: 3940-84-9
N-benzyl-3,4,5-trimethoxybenzamide

: 1430730-44-1
4-benzyl-5-(3,4,5-trimethoxyphenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 2 h / Reflux

2: m-xylene / 8 h / Reflux

With thionyl chloride; In m-xylene;

Reference yield:

: 4521-61-3
3,4,5-Trimethoxybenzoyl chloride

: 1430730-44-1
4-benzyl-5-(3,4,5-trimethoxyphenyl)-3-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosyl)-1,2,4-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: calcium chloride; triethylamine / 2 h / 0 - 20 °C

2: thionyl chloride / 2 h / Reflux

3: m-xylene / 8 h / Reflux

With thionyl chloride; triethylamine; calcium chloride; In m-xylene;
DOI:10.1016/j.ejmech.2014.02.041