diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfoxide

Base Information

Chemical Name:diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfoxide
CAS No.:216007-29-3
Molecular Formula:C₂₉H₂₉N₃O₆S₃
Molecular Weight:611.764
Hs Code.:

Synonyms:diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfoxide

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Chemical Property of diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfoxide

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Technology Process of diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfoxide

There total 4 articles about diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 216007-23-7
diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate

: 216007-29-3
diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfoxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform;
DOI:10.1021/jo970737f

Reference yield:

: 4104-47-6
N-sulfinyl-p-toluenesulfonamide

: 216007-29-3
diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfoxide

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / pyridine / benzene / Ambient temperature

2: 49 percent / CH₂Cl₂ / 0.08 h

3: 68 percent / Proton Sponge / CHCl₃ / 12 h / Ambient temperature

4: 62 percent / m-chloroperbenzoic acid / CHCl₃

With pyridine; Proton Sponge; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform; benzene;
DOI:10.1021/jo970737f

Reference yield:

: 851-06-9
bis(p-toluenesulfonyl) sulfur diimide

: 216007-29-3
diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfoxide

Guidance literature:: Multi-step reaction with 3 steps

1: 49 percent / CH₂Cl₂ / 0.08 h

2: 68 percent / Proton Sponge / CHCl₃ / 12 h / Ambient temperature

3: 62 percent / m-chloroperbenzoic acid / CHCl₃

With Proton Sponge; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform;
DOI:10.1021/jo970737f