diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfone

Base Information

Chemical Name:diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfone
CAS No.:216007-24-8
Molecular Formula:C₂₉H₂₉N₃O₇S₃
Molecular Weight:627.763
Hs Code.:

Synonyms:diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfone

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Chemical Property of diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfone

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Technology Process of diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfone

There total 5 articles about diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 216007-29-3
diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfoxide

: 216007-24-8
diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfone

Guidance literature:: With potassium permanganate; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; Ambient temperature;
DOI:10.1021/jo970737f

Reference yield:

: 4104-47-6
N-sulfinyl-p-toluenesulfonamide

: 216007-24-8
diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfone

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / pyridine / benzene / Ambient temperature

2: 49 percent / CH₂Cl₂ / 0.08 h

3: 68 percent / Proton Sponge / CHCl₃ / 12 h / Ambient temperature

4: 62 percent / m-chloroperbenzoic acid / CHCl₃

5: 63 percent / aq. KMnO₄, tetrabutylammonium hydrogen sulfate / CH₂Cl₂ / Ambient temperature

With pyridine; potassium permanganate; Proton Sponge; tetra(n-butyl)ammonium hydrogensulfate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform; benzene;
DOI:10.1021/jo970737f

Reference yield:

: 851-06-9
bis(p-toluenesulfonyl) sulfur diimide

: 216007-24-8
diphenylmethyl N-methyl-N-tosyl-S-aminosulfeniminopenicillanate-1-sulfone

Guidance literature:: Multi-step reaction with 4 steps

1: 49 percent / CH₂Cl₂ / 0.08 h

2: 68 percent / Proton Sponge / CHCl₃ / 12 h / Ambient temperature

3: 62 percent / m-chloroperbenzoic acid / CHCl₃

4: 63 percent / aq. KMnO₄, tetrabutylammonium hydrogen sulfate / CH₂Cl₂ / Ambient temperature

With potassium permanganate; Proton Sponge; tetra(n-butyl)ammonium hydrogensulfate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform;
DOI:10.1021/jo970737f