(1S,6R)-13-(Toluene-4-sulfonyl)-13-aza-tricyclo[7.7.0.0^1,6]hexadec-8-en-4-one

Base Information

Chemical Name:(1S,6R)-13-(Toluene-4-sulfonyl)-13-aza-tricyclo[7.7.0.0^1,6]hexadec-8-en-4-one
CAS No.:138831-95-5
Molecular Formula:C₂₂H₂₉NO₃S
Molecular Weight:387.543
Hs Code.:

(1S,6R)-13-(Toluene-4-sulfonyl)-13-aza-tricyclo[7.7.0.0<sup>1,6</sup>]hexadec-8-en-4-one

Synonyms:(1S,6R)-13-(Toluene-4-sulfonyl)-13-aza-tricyclo[7.7.0.0^1,6]hexadec-8-en-4-one

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Chemical Property of (1S,6R)-13-(Toluene-4-sulfonyl)-13-aza-tricyclo[7.7.0.0^1,6]hexadec-8-en-4-one

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Technology Process of (1S,6R)-13-(Toluene-4-sulfonyl)-13-aza-tricyclo[7.7.0.0^1,6]hexadec-8-en-4-one

There total 4 articles about (1S,6R)-13-(Toluene-4-sulfonyl)-13-aza-tricyclo[7.7.0.0^1,6]hexadec-8-en-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 138834-27-2
C₃₀H₄₉NO₅SSi

: 138831-95-5
(1S,6R)-13-(Toluene-4-sulfonyl)-13-aza-tricyclo[7.7.0.0^1,6]hexadec-8-en-4-one

Guidance literature:: With boron trifluoride diethyl etherate; In chloroform; Ambient temperature;
DOI:10.1016/0040-4039(91)80793-6

Reference yield:

: 70-55-3
toluene-4-sulfonamide

: 138831-95-5
(1S,6R)-13-(Toluene-4-sulfonyl)-13-aza-tricyclo[7.7.0.0^1,6]hexadec-8-en-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / n-Bu₄NI, NaOH / benzene; H₂O

2: 82 percent / BF₃*OEt₂ / CHCl₃ / Ambient temperature

With sodium hydroxide; boron trifluoride diethyl etherate; tetra-(n-butyl)ammonium iodide; In chloroform; water; benzene;
DOI:10.1016/0040-4039(91)80793-6

Reference yield:

: C₂₃H₄₄O₅Si

: 138831-95-5
(1S,6R)-13-(Toluene-4-sulfonyl)-13-aza-tricyclo[7.7.0.0^1,6]hexadec-8-en-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / -23 deg C to r. t.

2: 50 percent / n-Bu₄NI, NaOH / benzene; H₂O

3: 82 percent / BF₃*OEt₂ / CHCl₃ / Ambient temperature

With sodium hydroxide; boron trifluoride diethyl etherate; tetra-(n-butyl)ammonium iodide; triethylamine; In dichloromethane; chloroform; water; benzene;
DOI:10.1016/0040-4039(91)80793-6