α-carbonyl((diphenylphosphino)acetato-P,O)((diphenylphosphino)acetic acid-P)rhodium(I)

Base Information

Chemical Name:α-carbonyl((diphenylphosphino)acetato-P,O)((diphenylphosphino)acetic acid-P)rhodium(I)
CAS No.:92763-44-5
Molecular Formula:C₂₉H₂₅O₅P₂Rh
Molecular Weight:618.368
Hs Code.:

Synonyms:α-carbonyl((diphenylphosphino)acetato-P,O)((diphenylphosphino)acetic acid-P)rhodium(I)

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Chemical Property of α-carbonyl((diphenylphosphino)acetato-P,O)((diphenylphosphino)acetic acid-P)rhodium(I)

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Technology Process of α-carbonyl((diphenylphosphino)acetato-P,O)((diphenylphosphino)acetic acid-P)rhodium(I)

There total 3 articles about α-carbonyl((diphenylphosphino)acetato-P,O)((diphenylphosphino)acetic acid-P)rhodium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 92763-44-5
α-carbonyl((diphenylphosphino)acetato-P,O)((diphenylphosphino)acetic acid-P)rhodium(I)

: 113667-41-7,92763-44-5
γ-carbonyl((diphenylphosphino)acetato-P,O)((diphenylphosphino)acetic acid-P)rhodium(I)

Guidance literature:: In acetone; Rh-complex was dissolved in warm acetone, filtered, cooled to 10°C, mixed with toluene, vac. evapd. at 10°C under N2; filtered, washed with acetone;

Reference yield: 90.0%

: 92763-44-5
α-carbonyl((diphenylphosphino)acetato-P,O)((diphenylphosphino)acetic acid-P)rhodium(I)

: 113667-41-7,92763-44-5
β-carbonyl((diphenylphosphino)acetato-P,O)((diphenylphosphino)acetic acid-P)rhodium(I)

Guidance literature:: In water; acetone; Rh-complex was dissolved with heating in aq. acetone, filtered, soln. was vac. evapd. under N2; washed with aq. acetone, recrystd. from aq. acetone by evapn.;

Reference yield: 80.0%

: 15318-33-9,16353-77-8,13938-94-8
chlorocarbonylbis(triphenylphosphine)rhodium(I)

: 3064-56-0
diphenylphosphinoacetic acid

: 92763-44-5,113667-41-7
(diphenylphosphinoacetato)(diphenylphosphinoacetic acid)carbonylrhodium(I)

Guidance literature:: In benzene; under N2, refluxed for 2 h; filtered, washed with benzene, recrystn. (CHCl3/n-hexane); elem. anal.;
DOI:10.1016/S0020-1693(00)83686-5