(2R)-1,2-di-O-benzyl-3-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyl)glycerol

Base Information

Chemical Name:(2R)-1,2-di-O-benzyl-3-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyl)glycerol
CAS No.:58438-08-7
Molecular Formula:C₃₁H₃₈O₁₂
Molecular Weight:602.636
Hs Code.:

Synonyms:(2R)-1,2-di-O-benzyl-3-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyl)glycerol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-1,2-di-O-benzyl-3-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyl)glycerol

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Technology Process of (2R)-1,2-di-O-benzyl-3-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyl)glycerol

There total 12 articles about (2R)-1,2-di-O-benzyl-3-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyl)glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 20196-71-8
(2S)-2,3-bis(benzyloxy)propanol

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 58438-08-7
(2R)-1,2-di-O-benzyl-3-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyl)glycerol

Guidance literature:: With mercury(II) cyanide; mercury dibromide; In acetonitrile; at 20 ℃; for 0.5h;
DOI:10.1016/S0040-4020(01)82350-4

Reference yield: 79.0%

: 58530-76-0
(R)-2,3-dibenzyloxy-1-propanol

: 74808-10-9
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)trichloroacetimidate

: 58438-08-7
(2R)-1,2-di-O-benzyl-3-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyl)glycerol

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -15 - 0 ℃; for 4h; Molecular sieve;
DOI:10.1039/c4ob00721b

Reference yield: 52.0%

: 20196-71-8
(2S)-2,3-bis(benzyloxy)propanol

: 74808-10-9
O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)trichloroacetimidate

: 58438-08-7
(2R)-1,2-di-O-benzyl-3-O-(2′,3′,4′,6′-tetra-O-acetyl-β-D-glucopyranosyl)glycerol

Guidance literature:: (2S)-2,3-bis(benzyloxy)propanol; O-(2,3,4,6-Tetra-O-acetyl-α-D-glucopyranosyl)trichloroacetimidate; With N-iodo-succinimide; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 0.333333h;
DOI:10.1039/c5cc04773k