3-bromopropyl 2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-β-D-glucopyranoside

Base Information

Chemical Name:3-bromopropyl 2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-β-D-glucopyranoside
CAS No.:1300064-18-9
Molecular Formula:C₃₉H₄₉BrO₉Si
Molecular Weight:769.802
Hs Code.:

Synonyms:3-bromopropyl 2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-bromopropyl 2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-β-D-glucopyranoside

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Technology Process of 3-bromopropyl 2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-β-D-glucopyranoside

There total 7 articles about 3-bromopropyl 2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: C₃₈H₄₄Cl₃NO₉Si

: 627-18-9
1-bromo-3-propanol

: 1300064-18-9
3-bromopropyl 2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-β-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -40 ℃; for 1h; Inert atmosphere; Molecular sieve;
DOI:10.1039/c0cc05580h

Reference yield: 58.0%

: 1300064-13-4
phenyl 2,3,4-tri-O-benzoyl-1-thio-6-O-triisopropylsilyl-β-D-glucopyranoside

: 627-18-9
1-bromo-3-propanol

: 1300064-18-9
3-bromopropyl 2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-β-D-glucopyranoside

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; Dimethyldisulphide; trifluoromethylsulfonic anhydride; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere; Molecular sieve;
DOI:10.1039/c0cc05580h

Reference yield:

: C₂₁H₃₆O₅SSi

: 1300064-18-9
3-bromopropyl 2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine; dmap / Inert atmosphere

2.1: N-Bromosuccinimide / acetone / 0.5 h / 20 °C / Inert atmosphere

2.2: 21 h / Inert atmosphere

3.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / -40 °C / Inert atmosphere; Molecular sieve

With pyridine; dmap; N-Bromosuccinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; acetone;
DOI:10.1039/c0cc05580h