phenyl 2,3,4-tri-O-benzoyl-1-thio-6-O-triisopropylsilyl-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 2,3,4-tri-O-benzoyl-1-thio-6-O-triisopropylsilyl-β-D-glucopyranoside
CAS No.:1300064-13-4
Molecular Formula:C₄₂H₄₈O₈SSi
Molecular Weight:740.99
Hs Code.:

Synonyms:phenyl 2,3,4-tri-O-benzoyl-1-thio-6-O-triisopropylsilyl-β-D-glucopyranoside

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Chemical Property of phenyl 2,3,4-tri-O-benzoyl-1-thio-6-O-triisopropylsilyl-β-D-glucopyranoside

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Technology Process of phenyl 2,3,4-tri-O-benzoyl-1-thio-6-O-triisopropylsilyl-β-D-glucopyranoside

There total 5 articles about phenyl 2,3,4-tri-O-benzoyl-1-thio-6-O-triisopropylsilyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: C₂₁H₃₆O₅SSi

: 98-88-4
benzoyl chloride

: 1300064-13-4
phenyl 2,3,4-tri-O-benzoyl-1-thio-6-O-triisopropylsilyl-β-D-glucopyranoside

Guidance literature:: With pyridine; dmap; at 20 ℃; for 4h;
DOI:10.1002/anie.201403543

Reference yield:

: 4551-15-9
phenylthiotrimethylsilane

: 1300064-13-4
phenyl 2,3,4-tri-O-benzoyl-1-thio-6-O-triisopropylsilyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: zinc(II) iodide / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: water; triethylamine / methanol / 20 °C / Inert atmosphere

3: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

4: pyridine; dmap / Inert atmosphere

With pyridine; 1H-imidazole; dmap; water; triethylamine; zinc(II) iodide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c0cc05580h

Reference yield:

: 2936-70-1,5624-48-6,13992-15-9,16758-34-2,28244-97-5,77481-62-0,77481-63-1,105088-17-3,149495-84-1
(2R,3S,4S,5R,6S)-2-Hydroxymethyl-6-phenylsulfanyl-tetrahydro-pyran-3,4,5-triol

: 1300064-13-4
phenyl 2,3,4-tri-O-benzoyl-1-thio-6-O-triisopropylsilyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

2: pyridine; dmap / Inert atmosphere

With pyridine; 1H-imidazole; dmap; In N,N-dimethyl-formamide;
DOI:10.1039/c0cc05580h