4-phenoxy-N-methyl undecate-1,8-naphthalenediimide

Base Information

Chemical Name:4-phenoxy-N-methyl undecate-1,8-naphthalenediimide
CAS No.:1015814-14-8
Molecular Formula:C₃₀H₃₃NO₅
Molecular Weight:487.596
Hs Code.:

Synonyms:4-phenoxy-N-methyl undecate-1,8-naphthalenediimide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-phenoxy-N-methyl undecate-1,8-naphthalenediimide

Chemical Property:

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Technology Process of 4-phenoxy-N-methyl undecate-1,8-naphthalenediimide

There total 1 articles about 4-phenoxy-N-methyl undecate-1,8-naphthalenediimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1015814-15-9
4-bromo-N-methyl undecate-1,8-naphthalenediimide

: 108-95-2,27073-41-2
phenol

: 1015814-14-8
4-phenoxy-N-methyl undecate-1,8-naphthalenediimide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 8h; Inert atmosphere;
DOI:10.1039/b715462c

Reference yield: 83.0%

: 1015814-14-8
4-phenoxy-N-methyl undecate-1,8-naphthalenediimide

: 1252807-87-6
C₂₉H₃₁NO₅

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; for 72h;
DOI:10.1039/c3tc32158d

Reference yield:

: 1015814-14-8
4-phenoxy-N-methyl undecate-1,8-naphthalenediimide

: C₃₉H₄₂N₂O₆

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide; water / tetrahydrofuran / 72 h

2: dicyclohexyl-carbodiimide; benzotriazol-1-ol; triethylamine / dichloromethane / 12 h / Inert atmosphere; Reflux

With water; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; lithium hydroxide; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c3tc32158d