methyl 2--3-<2-bromo-4,5-(methylenedioxy)phenyl>propanoate

Base Information

• Chemical Name: methyl 2--3-<2-bromo-4,5-(methylenedioxy)phenyl>propanoate
• CAS No.: 147912-64-9
• Molecular Formula: C₃₀H₂₄BrNO₄
• Molecular Weight: 542.429

Synonyms:methyl 2--3-<2-bromo-4,5-(methylenedioxy)phenyl>propanoate

Chemical Property of methyl 2--3-<2-bromo-4,5-(methylenedioxy)phenyl>propanoate

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Technology Process of methyl 2--3-<2-bromo-4,5-(methylenedioxy)phenyl>propanoate

There total 2 articles about methyl 2--3-<2-bromo-4,5-(methylenedioxy)phenyl>propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

9-bromo-9-phenyl-9H-fluorene (55135-66-5) + methyl 2-amino-3-<2-bromo-4,5-(methylenedioxy)phenyl>propanoate hydrochloride → methyl 2--3-<2-bromo-4,5-(methylenedioxy)phenyl>propanoate (147912-64-9)

Guidance literature:

With potassium phosphate; lead(II) nitrate; In acetonitrile; Ambient temperature;

DOI:10.1021/jo00062a018

Reference yield:

5-bromo-6-bromomethylbenzo[1,3]dioxole (5434-47-9) → methyl 2--3-<2-bromo-4,5-(methylenedioxy)phenyl>propanoate (147912-64-9)

Guidance literature:

Multi-step reaction with 2 steps

2: 90 percent / Pb(NO₃)2, K₃PO₄ / acetonitrile / Ambient temperature

With potassium phosphate; lead(II) nitrate; In acetonitrile;

DOI:10.1021/jo00062a018

Reference yield: 95.0%

methyl 2--3-<2-bromo-4,5-(methylenedioxy)phenyl>propanoate (147912-64-9) → 2--3-<2-bromo-4,5-(methylenedioxy)phenyl>propanoic acid (147912-69-4)

Guidance literature:

With lithium hydroxide; In 1,4-dioxane; water; at 60 ℃; for 20h;

DOI:10.1021/jo00062a018

upstream raw materials:

9-bromo-9-phenyl-9H-fluorene

5-bromo-6-bromomethylbenzo[1,3]dioxole

Downstream raw materials:

2--3-<2-bromo-4,5-(methylenedioxy)phenyl>propanoic acid

6-(9-Phenyl-9H-fluoren-9-ylamino)-6,7-dihydro-indeno[5,6-d][1,3]dioxol-5-one

3-(9-phenylfluoren-9-yl)-4-<<2-bromo-4,5-(methylenedioxy)phenyl>methyl>oxazolidin-5-one

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