2-chloro-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

Base Information

Chemical Name:2-chloro-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone
CAS No.:150312-49-5
Molecular Formula:C₁₈H₁₉ClO₄
Molecular Weight:334.799
Hs Code.:

Synonyms:2-chloro-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

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Chemical Property of 2-chloro-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

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Technology Process of 2-chloro-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

There total 4 articles about 2-chloro-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 150312-48-4
8,8-dichloro-4-oxa-3-[2-(3,4,5-trimethoxyphenyl)ethyl]tricyclo[5.1.0.0^3,5]octan-1-ol

: 150312-49-5
2-chloro-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 5h; Heating;
DOI:10.1016/S0968-0896(02)00052-4

Reference yield:

: 731849-14-2
7,7-dichloro-3-[2-(3,4,5-trimethoxyphenyl)ethyl]bicyclo[4.1.0]hept-3-en-1-ol

: 150312-49-5
2-chloro-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / MCPBA / CH₂Cl₂ / 3.5 h / 20 °C

2: 57 percent / p-toluenesulfonic acid / benzene / 5 h / Heating

With toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;
DOI:10.1016/S0968-0896(02)00052-4

Reference yield:

: 150312-47-3
1,1,2,2-tetramethyl-1-sila-1-{5-[2-(3,4,5-trimethoxyphenyl)ethyl]cyclohexa-1,4-dienyloxy}propane

: 150312-49-5
2-chloro-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,2-dimethoxy-ethane / 5 h / Heating

1.2: 53 percent / 20 percent HF / acetonitrile / 12 h / 20 °C

2.1: 67 percent / MCPBA / CH₂Cl₂ / 3.5 h / 20 °C

3.1: 57 percent / p-toluenesulfonic acid / benzene / 5 h / Heating

With toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In 1,2-dimethoxyethane; dichloromethane; benzene;
DOI:10.1016/S0968-0896(02)00052-4