2-methoxy-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

Base Information

Chemical Name:2-methoxy-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone
CAS No.:150312-43-9
Molecular Formula:C₁₉H₂₂O₅
Molecular Weight:330.381
Hs Code.:

Synonyms:2-methoxy-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

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Chemical Property of 2-methoxy-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

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Technology Process of 2-methoxy-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

There total 5 articles about 2-methoxy-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 67-56-1
methanol

: 150312-49-5
2-chloro-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

: 150312-43-9
2-methoxy-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

Guidance literature:: methanol; With iodine; magnesium; for 1h; Heating;

2-chloro-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone; at 20 ℃; for 7.5h;
DOI:10.1016/S0968-0896(02)00052-4

Reference yield:

: 731849-14-2
7,7-dichloro-3-[2-(3,4,5-trimethoxyphenyl)ethyl]bicyclo[4.1.0]hept-3-en-1-ol

: 150312-43-9
2-methoxy-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

Guidance literature:: Multi-step reaction with 3 steps

1.1: 67 percent / MCPBA / CH₂Cl₂ / 3.5 h / 20 °C

2.1: 57 percent / p-toluenesulfonic acid / benzene / 5 h / Heating

3.1: Mg; I₂ / 1 h / Heating

3.2: 66 percent / 7.5 h / 20 °C

With iodine; toluene-4-sulfonic acid; magnesium; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;
DOI:10.1016/S0968-0896(02)00052-4

Reference yield:

: 150312-48-4
8,8-dichloro-4-oxa-3-[2-(3,4,5-trimethoxyphenyl)ethyl]tricyclo[5.1.0.0^3,5]octan-1-ol

: 150312-43-9
2-methoxy-6-[2-(3,4,5-trimethoxy-phenyl)-ethyl]-cyclohepta-2,4,6-trienone

Guidance literature:: Multi-step reaction with 2 steps

1.1: 57 percent / p-toluenesulfonic acid / benzene / 5 h / Heating

2.1: Mg; I₂ / 1 h / Heating

2.2: 66 percent / 7.5 h / 20 °C

With iodine; toluene-4-sulfonic acid; magnesium; In benzene;
DOI:10.1016/S0968-0896(02)00052-4