(3R,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

Base Information

Chemical Name:(3R,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal
CAS No.:566949-64-2
Molecular Formula:C₃₁H₅₈O₅Si₂
Molecular Weight:566.97
Hs Code.:

Synonyms:(3R,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

Suppliers and Price of (3R,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3R,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3R,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

There total 4 articles about (3R,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 566949-63-1
(3R,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methyl-N,N-diethylbutanamide

: 566949-64-2
(3R,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

Guidance literature:: With diisobutylaluminium hydride; In diethyl ether; toluene; at 0 ℃; for 2h;
DOI:10.1039/b211801g

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 566949-64-2
(3R,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 °C

2: 85 percent / AlMe₃ / CH₂Cl₂; hexane / 16 h / 20 °C

3: 83 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 °C

4: 58 percent / DIBAL-H / diethyl ether; toluene / 2 h / 0 °C

With 2,6-dimethylpyridine; trimethylaluminum; diisobutylaluminium hydride; In diethyl ether; hexane; dichloromethane; toluene;
DOI:10.1039/b211801g

Reference yield:

: 566949-61-9
(3R)-3-[(S)-(3,4-dimethoxyphenyl)(triisopropylsilyloxy)methyl]-4-butanolide

: 566949-64-2
(3R,4S)-4-(3,4-dimethoxyphenyl)-4-(triisopropylsilyloxy)-3-(triisopropylsilyloxy)methylbutanal

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / AlMe₃ / CH₂Cl₂; hexane / 16 h / 20 °C

2: 83 percent / 2,6-lutidine / CH₂Cl₂ / 1 h / 0 °C

3: 58 percent / DIBAL-H / diethyl ether; toluene / 2 h / 0 °C

With 2,6-dimethylpyridine; trimethylaluminum; diisobutylaluminium hydride; In diethyl ether; hexane; dichloromethane; toluene;
DOI:10.1039/b211801g