Technology Process of C13H15NO3
There total 4 articles about C13H15NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
methyllithium lithium bromide; 2-(hydroxymethyl)benzenecorbonitrile;
In
diethyl ether;
at 0 ℃;
for 2h;
Inert atmosphere;
acetic anhydride;
In
diethyl ether;
at 20 ℃;
Inert atmosphere;
DOI:10.1039/c4cc04072d
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / benzene / 1 h / 80 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C
3.1: water; potassium carbonate / methanol / 20 °C
4.1: diethyl ether / 2 h / 0 °C / Inert atmosphere
4.2: 20 °C / Inert atmosphere
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); water; potassium carbonate;
In
methanol; diethyl ether; N,N-dimethyl-formamide; benzene;
DOI:10.1039/c4cc04072d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C
2.1: water; potassium carbonate / methanol / 20 °C
3.1: diethyl ether / 2 h / 0 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
With
water; potassium carbonate;
In
methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1039/c4cc04072d