Technology Process of C36H56O7Si2
There total 7 articles about C36H56O7Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
1,2-dichloro-benzene;
at 250 ℃;
Microwave irradiation;
DOI:10.1038/nchem.1074
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: diisobutylaluminium hydride / toluene / -78 °C
1.2: -78 - 20 °C
2.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C
3.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0 - 20 °C
4.1: isopropyl alcohol / 80 °C
5.1: 122 °C / neat (no solvent)
5.2: 20 °C
6.1: 1,2-dichloro-benzene / 250 °C / Microwave irradiation
With
carbon tetrabromide; sodium hydride; diisobutylaluminium hydride; triphenylphosphine;
In
dichloromethane; N,N-dimethyl-formamide; 1,2-dichloro-benzene; isopropyl alcohol; toluene;
5.1: Claisen rearrangement;
DOI:10.1038/nchem.1074
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C
2.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0 - 20 °C
3.1: isopropyl alcohol / 80 °C
4.1: 122 °C / neat (no solvent)
4.2: 20 °C
5.1: 1,2-dichloro-benzene / 250 °C / Microwave irradiation
With
carbon tetrabromide; sodium hydride; triphenylphosphine;
In
dichloromethane; N,N-dimethyl-formamide; 1,2-dichloro-benzene; isopropyl alcohol;
4.1: Claisen rearrangement;
DOI:10.1038/nchem.1074
