carbonic acid 4-nitrophenyl ester (2S,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester

Base Information

Chemical Name:carbonic acid 4-nitrophenyl ester (2S,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester
CAS No.:1181215-13-3
Molecular Formula:C₁₆H₂₁NO₉
Molecular Weight:371.344
Hs Code.:

Synonyms:carbonic acid 4-nitrophenyl ester (2S,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester

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Chemical Property of carbonic acid 4-nitrophenyl ester (2S,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester

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Technology Process of carbonic acid 4-nitrophenyl ester (2S,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester

There total 1 articles about carbonic acid 4-nitrophenyl ester (2S,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 14187-51-0
(3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyltetrahydro-2H-pyran-2-ol

: 7693-46-1
4-Nitrophenyl chloroformate

: 1181215-13-3
carbonic acid 4-nitrophenyl ester (2S,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester

: carbonic acid 4-nitrophenyl ester (2R,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester

Guidance literature:: With pyridine; In 1,4-dioxane; at 20 ℃; Cooling with ice;

Reference yield: 29.0%

: 1181214-69-6
4-[2-(4-trifluoromethyl-phenyl)-pyrimidin-4-yl]-phenylamine

: 1181215-13-3
carbonic acid 4-nitrophenyl ester (2S,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester

: 1181213-45-5
{4-[2-(4-trifluoromethylphenyl)-pyrimidin-4-yl]-phenyl}-carbamic acid (2S,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester

Guidance literature:: 4-[2-(4-trifluoromethyl-phenyl)-pyrimidin-4-yl]-phenylamine; With potassium hexamethylsilazane; In toluene; Cooling with ice;

carbonic acid 4-nitrophenyl ester (2S,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester; In toluene; at 20 ℃; Cooling with ice;

Reference yield: 8.0%

: 1181215-14-4
4-[2-(4-methoxyphenyl)-pyrimidin-4-yl]-phenylamine

: 1181215-13-3
carbonic acid 4-nitrophenyl ester (2S,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester

: 1181213-47-7
{4-[2-(4-methoxyphenyl)-pyrimidin-4-yl]-phenyl}-carbamic acid (2S,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester

Guidance literature:: 4-[2-(4-methoxyphenyl)-pyrimidin-4-yl]-phenylamine; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; Cooling with ice;

carbonic acid 4-nitrophenyl ester (2S,3R,4R,5S,6S)-3,4,5-trimethoxy-6-methyl-tetrahydropyran-2-yl ester; In tetrahydrofuran; toluene; at 20 ℃; Cooling with ice;