4,4'-bis(2-tert-butyldiphenylsilyloxybenzyl)-2,2'-methylene dimethoxy phenol

Base Information

Chemical Name:4,4'-bis(2-tert-butyldiphenylsilyloxybenzyl)-2,2'-methylene dimethoxy phenol
CAS No.:197805-75-7
Molecular Formula:C₆₁H₆₄O₄Si₂
Molecular Weight:917.348
Hs Code.:

Synonyms:4,4'-bis(2-tert-butyldiphenylsilyloxybenzyl)-2,2'-methylene dimethoxy phenol

Suppliers and Price of 4,4'-bis(2-tert-butyldiphenylsilyloxybenzyl)-2,2'-methylene dimethoxy phenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,4'-bis(2-tert-butyldiphenylsilyloxybenzyl)-2,2'-methylene dimethoxy phenol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,4'-bis(2-tert-butyldiphenylsilyloxybenzyl)-2,2'-methylene dimethoxy phenol

There total 5 articles about 4,4'-bis(2-tert-butyldiphenylsilyloxybenzyl)-2,2'-methylene dimethoxy phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 77-78-1
dimethyl sulfate

: 197805-69-9
4,4'-bis(2-tert-butyldiphenylsilyloxybenzyl)-2,2'-methylenediphenol

: 197805-75-7
4,4'-bis(2-tert-butyldiphenylsilyloxybenzyl)-2,2'-methylene dimethoxy phenol

Guidance literature:: With potassium carbonate; In acetone; for 23.5h; Heating;
DOI:10.1016/S0040-4020(97)00903-4

Reference yield:

: 2467-03-0
2-[(4-hydroxyphenyl)methyl]phenol

: 197805-75-7
4,4'-bis(2-tert-butyldiphenylsilyloxybenzyl)-2,2'-methylene dimethoxy phenol

Guidance literature:: Multi-step reaction with 5 steps

1: 65 percent / imidazole / dimethylformamide / 1 h / Ambient temperature

2: 98 percent / imidazole / dimethylformamide / 24 h

3: 86 percent / BF₃*OEt₂ / CHCl₃ / 17 h / 0 °C

4: 1.) EtMgBr / 1.) Et₂O, 25 deg C, 30 min, 2.) C₆H₆, reflux, 20.5 h

5: 58 percent / K₂CO₃ / acetone / 23.5 h / Heating

With 1H-imidazole; boron trifluoride diethyl etherate; ethylmagnesium bromide; potassium carbonate; In chloroform; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4020(97)00903-4

Reference yield:

: 197805-63-3
2-[4-(tert-Butyl-dimethyl-silanyloxy)-benzyl]-phenol

: 197805-75-7
4,4'-bis(2-tert-butyldiphenylsilyloxybenzyl)-2,2'-methylene dimethoxy phenol

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / imidazole / dimethylformamide / 24 h

2: 86 percent / BF₃*OEt₂ / CHCl₃ / 17 h / 0 °C

3: 1.) EtMgBr / 1.) Et₂O, 25 deg C, 30 min, 2.) C₆H₆, reflux, 20.5 h

4: 58 percent / K₂CO₃ / acetone / 23.5 h / Heating

With 1H-imidazole; boron trifluoride diethyl etherate; ethylmagnesium bromide; potassium carbonate; In chloroform; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4020(97)00903-4