4'-Methyl-N-methyl-mandelanilid; DL-Mandelsaeure-

Base Information

Chemical Name:4'-Methyl-N-methyl-mandelanilid; DL-Mandelsaeure-
CAS No.:20423-84-1
Molecular Formula:C₁₆H₁₇NO₂
Molecular Weight:255.316
Hs Code.:

4'-Methyl-N-methyl-mandelanilid; DL-Mandelsaeure-<N-methyl-p-toluidid>

Synonyms:4'-Methyl-N-methyl-mandelanilid; DL-Mandelsaeure-

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Chemical Property of 4'-Methyl-N-methyl-mandelanilid; DL-Mandelsaeure-

Chemical Property:

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Technology Process of 4'-Methyl-N-methyl-mandelanilid; DL-Mandelsaeure-

There total 7 articles about 4'-Methyl-N-methyl-mandelanilid; DL-Mandelsaeure- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1335242-84-6
N-methyl-2-oxo-2-phenyl-N-(p-tolyl)acetamide

: 20423-84-1
4'-Methyl-N-methyl-mandelanilid; DL-Mandelsaeure-

Guidance literature:: N-methyl-2-oxo-2-phenyl-N-(p-tolyl)acetamide; With sodium tetrahydroborate; In ethanol; dichloromethane; at 20 ℃; Cooling with ice;

With water; ammonium chloride; In ethanol; dichloromethane;
DOI:10.1021/ja1027327

Reference yield:

: 15206-55-0
methyl 2-oxo-2-phenylacetate

: 20423-84-1
4'-Methyl-N-methyl-mandelanilid; DL-Mandelsaeure-

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / water / 20 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 0 - 20 °C

2.2: 0 - 20 °C

3.1: sodium tetrahydroborate / methanol / 0 - 20 °C

With sodium tetrahydroborate; oxalyl dichloride; sodium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1055/a-1373-7017

Reference yield:

: 4358-87-6
(RS)-methyl mandelate

: 20423-84-1
4'-Methyl-N-methyl-mandelanilid; DL-Mandelsaeure-

Guidance literature:: Multi-step reaction with 4 steps

1.1: manganese(IV) oxide / dichloromethane / 20 °C

2.1: sodium hydroxide / water / 20 °C

3.1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 0 - 20 °C

3.2: 0 - 20 °C

4.1: sodium tetrahydroborate / methanol / 0 - 20 °C

With manganese(IV) oxide; sodium tetrahydroborate; oxalyl dichloride; sodium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1055/a-1373-7017