[4-(1,3-benzothiazol-2-yl)-2-nitrophenyl](2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone

Base Information

Chemical Name:[4-(1,3-benzothiazol-2-yl)-2-nitrophenyl](2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone
CAS No.:1370531-42-2
Molecular Formula:C₂₃H₂₅N₃O₃S₃
Molecular Weight:487.668
Hs Code.:

Synonyms:[4-(1,3-benzothiazol-2-yl)-2-nitrophenyl](2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone

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Chemical Property of [4-(1,3-benzothiazol-2-yl)-2-nitrophenyl](2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone

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Technology Process of [4-(1,3-benzothiazol-2-yl)-2-nitrophenyl](2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone

There total 11 articles about [4-(1,3-benzothiazol-2-yl)-2-nitrophenyl](2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₇ClN₂O₃S

: 105089-88-1
(2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-pyrrole

: 1370531-42-2
[4-(1,3-benzothiazol-2-yl)-2-nitrophenyl](2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 1.5h;
DOI:10.1016/j.ejmech.2012.01.014

Reference yield:

: 96-98-0
4-methyl-3-nitrobenzoic acid

: 1370531-42-2
[4-(1,3-benzothiazol-2-yl)-2-nitrophenyl](2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone

Guidance literature:: Multi-step reaction with 7 steps

1: thionyl chloride; N,N-dimethyl-formamide / benzene / 80 °C

2: triethylamine / tetrahydrofuran / 0 - 20 °C

3: Lawessons reagent / toluene / 60 °C / Reflux

4: Dess-Martin periodane / dichloromethane / 20 °C

5: pyridine; tetra-n-butylammonium permanganate / 12 h / 20 °C

6: thionyl chloride; N,N-dimethyl-formamide / benzene / Reflux

7: triethylamine / tetrahydrofuran / 1.5 h / 0 - 20 °C

With Lawessons reagent; pyridine; thionyl chloride; tetra-n-butylammonium permanganate; Dess-Martin periodane; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; toluene; benzene;
DOI:10.1016/j.ejmech.2012.01.014

Reference yield:

: 1370531-38-6
4-(1,3-benzothiazol-2-yl)-2-nitrobenzoic acid

: 1370531-42-2
[4-(1,3-benzothiazol-2-yl)-2-nitrophenyl](2S)-2-[di(ethylsulfanyl)methyl]tetrahydro-1H-1-pyrrolylmethanone

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; N,N-dimethyl-formamide / benzene / Reflux

2: triethylamine / tetrahydrofuran / 1.5 h / 0 - 20 °C

With thionyl chloride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; benzene;
DOI:10.1016/j.ejmech.2012.01.014